Pre lab 17

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Salt Lake Community College *

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2310

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Chemistry

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Dec 6, 2023

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pdf

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10/11/23, 8:41 PM CHM 2211L - Broward College-Central : Experiment 17: Pre-Lab Questions https://bookshelf.vitalsource.com/reader/books/9781533939012/epubcfi/6/36[%3Bvnd.vst.idref%3Drefid-6b2b895f-763e-4c76-8f20-e3857f9f59e6]!/4/6[6b2b895f-7… 1/3 Write your name , date , and section in the block below: Valentina Espinosa Canon 10/11/23 SDBS, National Institute of Advanced Industrial Science and Technology 1. For the above compound, assign the IR bands which are useful in assigning the molecular structure. The Carbonyl stretch appears at around 1720 cm^-1 The C=C appears at around 1640 cm^-1 Experiment 17: Pre-Lab Questions Due before lab begins. Answer in space provided.
10/11/23, 8:41 PM CHM 2211L - Broward College-Central : Experiment 17: Pre-Lab Questions https://bookshelf.vitalsource.com/reader/books/9781533939012/epubcfi/6/36[%3Bvnd.vst.idref%3Drefid-6b2b895f-763e-4c76-8f20-e3857f9f59e6]!/4/6[6b2b895f-7… 2/3 SDBS, National Institute of Advanced Industrial Science and Technology 2. For the above compound, assign the IR bands which are useful in assigning the molecular structure. the carbonyl stretch at around 1730 cm^-1 3. For each of the following compounds, predict the IR bands useful in assigning the molecular structure. 2-Pentatone Heptanal 2-Ethylbutanoic Acid 1.) 2- pentatone for the C=O A strong peak between 1690-1715 cm^-1 C-H stretch around 2850-2950 cm^-1 2.) Heptanal C=O a stretch between 1700-1750 cm^-1 C-H stretch between 2800 - 3000 cm^-1 O-
10/11/23, 8:41 PM CHM 2211L - Broward College-Central : Experiment 17: Pre-Lab Questions https://bookshelf.vitalsource.com/reader/books/9781533939012/epubcfi/6/36[%3Bvnd.vst.idref%3Drefid-6b2b895f-763e-4c76-8f20-e3857f9f59e6]!/4/6[6b2b895f-7… 3/3 H Stretch between 3250-3600 cm^-1 3.) 2-Ethylbutanoic Acid C=O Stretch: A peak around 1690-1720 cm^-1 O-H Stretch: A broad peak ibetwen 3200-3600 cm^-1. C-H Stretch: Stretch around 2800-3000 cm^-1 4. For each of the following compounds in the table below, predict the NMR signals which are expected to be useful in assigning the molecular structure. Predict the approximate chemical shift and the splitting pattern. 3-Methoxyaniline 4-Isopropoxybenzoic Acid 2-Pentanone Allyl Hexanoate Heptanal 2-Ethylbutanoic Acid
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