Nick's Final Exam Orgo Lab

.pdf

School

Florida International University *

*We aren’t endorsed by this school

Course

2210L

Subject

Chemistry

Date

Dec 6, 2023

Type

pdf

Pages

6

Uploaded by EarlMetalCaterpillar32

Report
CHM 2210L Section: ______________________ TA: ________________________________________ Name: ___________________________________ Panther ID: _____________________ Points total: __________/100
1. What is the significance of a small melting point range (within 2 degrees) in comparison to a large melting point range? (5 points) a) melting point range holds no significance b) A large melting point range shows that the substance was pure c) A small melting point range show that the substance was pure d) A small melting point range shows that the substance has impurities 2. Why would you use fractional distillation instead of simple distillation? (5 points) a. If the melting point difference of the liquids is greater than 80 apart b. If the boiling point difference of the liquids is greater than 80 apart c. If the melting point difference of the liquids is less than 80 apart d. If the boiling point difference of the liquids is less than 80 apart 3. Label the apparatus with the following terms below: (10 points) a. Funnel b. Metal Ring c. Flask d. Stopcock e. Stand
4. You are conducting a recrystallization in which 1.40g recrystallized and the theoretical yield is 1.83g. Calculate the percent yield: (5 points) a) 77% b) 89% c) 140% d) 29% 5. When should you use hot filtration instead of vacuum filtration? (5 points) a) To filter solutions that will crystallize when allowed to cool b) To filter solutions that are liquid c) To filter solutions that are insoluble in solution d) To filter solutions that have a high boiling point 6. The purpose of releasing the stopper while shaking the separatory funnel is to _____ (5 points) a) Allow the water to combine with the aqueous solution b) Give the liquids a break c) Relieve the pressure in the separatory funnel d) Dissolve the solids in the liquid solution 7. The distance traveled by a solute in TLC chromatography is 0.45 and the distance traveled by solvent was 0.53. Calculate the Rf value: (5 points) a) 0.85 b) 0.57 c) 1.23 d) 0.36
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