Starch Assignment (2)
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Wayne State University *
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Chemistry
Date
Apr 3, 2024
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Name: Valeria Diaz
Lab Report: Starch
I
nstructions
Step 1:
After reading the lab manual and powerpoint, and watching the video provided on Canvas, complete the following table. (5 points) Step 2:
Answer the study questions. Please answer questions thoroughly. (5 points) After completing the lab based on the lab manual instructions and watching the lab video provided on canvas, answer the following questions. After performing Agitation and temperature effect on the smoothness of the paste (Part 1) of the procedures:
1.
describe the consistency of the sol from the procedure A-C based on the experiment. 2.
Describe only the appearance
of each corn starch pastes after performing part 2 of the procedures and after watching the video titled “Starch Video” under modules. This is a YouTube video. Starch
Appearance
Potato Starch a thickened gel
Waxy Rice Starch liquid, cloudy
Rice Starch liquid cloudy
Corn Starch 16g
thickened liquid
Corn Starch 8g
semi-thick liquid
Tapioca Starch
clear, semi-jelly
3.
Use part 3 of the procedures to perform a cold line spread and provide the average of each sample given in the video. Starch
Cold Line Spread
L
M
N
O
P
Study Questions:
1.
Why do some experiments form lumps in the starch paste during the process (refer to results from part 1 of the procedures in the lab manual)?
Starch clumps tend to clump together due it being hydrophobic
2.
Describe how the amylose content affects the properties of starch paste (refer to the lab manual).
It can affect the texture of the paste
3.
Provide examples of starch that are suitable for making thick soups.
Cornstarch is typically the best for making thick soups
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Related Questions
read the Procedure and answer the post lab questions below:
Using a balance, mass between 1.50 – 2.00 grams of sodium carbonate in a pre-massed 150mL beaker.
Add 20 mL of distilled water and stir thoroughly to make sure all the crystals are dissolved. Rinse the stirring rod with a little distilled water after stirring.
Using a balance, mass between 1.50 – 2.00 grams of calcium chloride dihydrate in a pre-massed 50 mL beaker.
Repeat Step 2 for the solution in the 50 mL beaker.
Pour the calcium chloride solution into the 150mL beaker containing the sodium carbonate solution and stir.
Mass a piece of filter paper. Fold the filter paper and place it into the funnel. Wet it with a little distilled water to ensure that it is stuck to the sides of the funnel.
Slowly pour the mixture from the beaker into the funnel and collect the filtrate into a 125mL erlenmeyer flask. Do not allow the mixture to rise above the edge of the filter paper.
Rinse the beaker with about 10 mL of distilled water.…
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read the Procedure and answer the post lab questions below:
Using a balance, mass between 1.50 – 2.00 grams of sodium carbonate in a pre-massed 150mL beaker.
Add 20 mL of distilled water and stir thoroughly to make sure all the crystals are dissolved. Rinse the stirring rod with a little distilled water after stirring.
Using a balance, mass between 1.50 – 2.00 grams of calcium chloride dihydrate in a pre-massed 50 mL beaker.
Repeat Step 2 for the solution in the 50 mL beaker.
Pour the calcium chloride solution into the 150mL beaker containing the sodium carbonate solution and stir.
Mass a piece of filter paper. Fold the filter paper and place it into the funnel. Wet it with a little distilled water to ensure that it is stuck to the sides of the funnel.
Slowly pour the mixture from the beaker into the funnel and collect the filtrate into a 125mL erlenmeyer flask. Do not allow the mixture to rise above the edge of the filter paper.
Rinse the beaker with about 10 mL of distilled water.…
arrow_forward
Color BEFORE adding
Color AFTER adding
Intensity of color AFTER
adding FeCl3
Test Tube #
FeCl3
FeCl3
#1 (salicylic acid)
clear
lilac
100%
#2 (commercial aspirin A) clear
slightly pink
50%
#3 (commercial aspirin B) clear
lilac
95%
#4 (aspirin from your
clear
pink
20%
synthesis above)
#5 (control)
clear
clear
0%
Based on this data and the melting point of Aspirin, how pure is the synthesized product?
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1.
Component
Container
Stretch Wrap
Pallet
Product
Material
Polypropylene
Polystyrene
Wood
Ca(OCI)2
Weight (kg/pallet)
48
0.5
15-18
725
Based on the above table, answer the following questions.
(a) Discuss the possibility of fire at the calcium hypochlorite Ca(OCI)2 storage warehouse. Include your assumption on how the fire could spread in the storage warehouse.
(b) Recommend solutions to avoid fire occur at the storage warehouse.
(10)
(10)
(Total / Jumlah: 20 )
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A sample of rainwater was collected from four separate locations across theMetroplex. Each sample was measured once by two separate methods for the presence ofsulfate. Determine whether the two methods are equivalent with respect to giving thesame answer for [SO42-].
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Soil Lab 11a Direct Measurement of Soil Porosity
1. Fill a 100 ml graduated cylinder to the 100 ml mark with tap water. Tilt the beaker containing the
soil sąved from Step 3 in the Bulk Density Determination to about a 45 degree angle. Pour the water
very slowly onto the soil in the beaker. Stop adding water when the soil pores are filled (saturated)
and the soil surface glistens.
2. Allow the soil to stand for several minutes to make sure the water has filled the very small soil pores.
Any excess water can be returned to the graduated cylinder. Don't stir or shake the mixture.
3. Determine the amouht of water used to exactly fill the pote space in the 100 cubic cehtimeters of
soil. Subtrąct the reading of water level on the side of the graduated cylinder from the original
volume of 100 ml. Note that the water which was poured onto the soil exactly filled the pore space
and thus equals the total pore volume by direct measurement.
4. Record your results below and make the necessary…
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A supporting electrolyte is usually added to the analyte solution to
minimize solution resistance.minimize solution conductivity.make the analyte less soluble in solution.increase the scan rate.
arrow_forward
Data Table 1
Enter the calculated molarity and measured conductivity values in the table.
Data Table 1: Experimental Data
Sodium
Total
Sodium Chloride
Standard Chloride Volume Concentration (M or Conductivity (µS)
(g)
(mL)
mol/L)
Blank
100.00
8.965
A
0.0059 100.00
В
0.0531 100.00
0.1029 100.00
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PART 3- LABORATORY EQUIPMENT
EQUIPMENT NAME
FUNCTION
To hold test tubes.
Attaches to a retort stand to support glassware being heated.
To pour liquid from a large container into a small container.
To provide a flame during an experiment.
ones
To light the Bunsen burner.
To attach test tubes to a retort stand.
To clean substances out of a test tube.
To hold a hot crucible or flask.
To hold a hot test tube.
To place on the lab bench to prevent burning or to use with ring clamp.
To transfer small amounts of liquid.
To grow bacteria or contain small experiments.
To hold liquids.
To measure liquids.
To contain experiments (a stopper can be used to close the flask).
To hold a hot beaker.
To perform an experiment with a different substance in each well.
To hold chemicals and perform experiments in.
To scoop and transfer small amounts of substances,
To stir during experiments that involve mixing or dissolving.
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Please answser 18-19-20
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A gram of soil sample as received contains 15.00% water. After oven drying to remove the mixture, it was found to contain 16.00% K. Find the %K in the original sample as received.
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Volumetric pipettes are designed to deliver a precise amount of liquid, but only if you
a. submerge the end of the pipette into a solution you are delivering.
b. allow the pipette to drain freely, and leave any residual solution in the pipette.
c. hold the pipette at a 45 degree angle and ensure that all the liquid is delivered.
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Aromatic Water
Peppermint water (Simple solution method)
Formula
Peppermint ol
Purifiled water.
To make 60ml
Materlals: Erlenmeyer flask, filtor paper
Procedure
Cinnamon water (Alternate solution method)
Formula
Cinnamon oil
Purified water
To make 60ml
Materials: Purified talc Erlenmeyer flask, filter paper
Procedure
Camphor water (Alternate solution method with trituration with intervention)
Formula
Camphor crystals
Purifled water
To make 60ml
Materials: 95% ethanol talc
mortar and pestle. Erlenmeyer flask, filter paper
Procedure
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Assume the data below was collected for two different sample solutions using the same
experimental procedure you carried out. Based on the two lines shown below, which
solution (orange data points or blue data points) corresponds to the sample with the
higher molar absorptivity?
0.9
y4.771 - 0.0728
0.7
0.6
04
0.3
02
y1414 - 0.0546
R0.99642
0.1
0.02
0.04
0.06
0.08
0.1
0.12
0.14
0.16
0.18
02
0.1
[Concentration, M]
orange data points (lower line)
O blue data points (upper line)
Absorbance
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Just prior to drying an organic layer with a drying agent, you notice water droplets in the organic
layer. What should you do next?
Double the amount of drying agent used.
O Transfer the organic layer to a clean flask before adding any drying agent.
Stir or swirl with solution with the drying agent well.
Double the drying period and let the solution dry for 30 minutes.
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Unknown
Mixture #1
Unknown
Mixture #2
Sample
caffeine
ibuprofen
aspirin
acetaminoph
en
Distance to
solvent front
14,70 cm 14,70cm
14.70cm1u.70 cm
1나,구 cm
|14.구0cm
5. 70 cm
11.90 cm
I.85cm
Distance
Spot(s) traveled 175 cm
13.75cm
11.9 5 cm 6.4 0 cm
13,75 cm
13.75 cm
38 78
1908
.8095
Calculated R:(s)
119
,9354
812 9
43 S
.9354
9354
#1:Aspirin
an d lbuprofen
Components of
Unknowns
#2: Ace taminophen, aspirin
an d ibu profen
D. Additional Exercises
1. Which of the substances tested is most polar? What parts of the structure of this substance is polar?
The Sul
2. Which of the substance tested is most non-polar? What parts of the structure of this substance in non-polar?
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Table 2: Absorbance Values of Standards and Unknowns.
Sample
Blank
Standard Solution 1
Standard Solution 2
Standard Solution 3
Standard Solution 4
Standard Solution 5
Water Sample 1
Water Sample 2
Phosphate Concentration
(in ppm)
Y17
0 ppm
0.02 ppm
0.04 ppm
0.08 ppm
0.16 ppm
0.32 ppm
Freeman Lake
0.001
0.325
0.292
0.413
0.315
0.039
0.054
0.049
Absorbance at
2= 690 nm
Calculations:
1. Construct a phosphate standard curve in Excel by plotting concentration (in ppm) on your
x-axis and Absorbance (unitless) on your y-axis for your known solutions. Label the axes
on the graph and provide the curve with a title. Use a linear trendline to generate a best fit
line to your data. Label the graph with the equation and the R" value. Insert your labeled
graph in the space below.
X
arrow_forward
Nitrous Acid Test
Procedure: Make a solution of 4 grams NaNO3 in 16 mL water. Put 2 mL of concentrated hydrochloric acid into a 10x75-mm test tube and add 0.5 ml of amine. Cool the solution in a water-ice slush to zero degrees celcius. Add the nitrile solution slowly, dropwise, until a drop of the reaction mixture gives a blue spot on starch-iodide paper.
The following should be tested: (NOTE: Include the observations and reaction equation)
A. PRIMARY ALIPHATIC AMINES (Like Butylamine of Cyclohexylamine)
B. PRIMARY AROMATIC AMINES
I. Aniline + nitrous acid; then heat.
II. Aniline + nitrous acid; then B-Napthol.
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Carla is using a fertilizer that contains nitric acid. How is nitric acid classified?
strong acid
weak acid
strong base
weak base
Save and Exit
Next
Mark this and return
ContentViewers/AssessmentViewer/Activit.
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Table of chemicals and reagents with their physicochemical properties (name,
molecular formula, molecular weight, pKa, melting point, boiling point, etc.)
Write a short outline or a flow diagram of the procedure
List and safety issues
Read and understand the MSDS information for each chemical used in this practical
Experimental procedure
Please do not scratch the clear sides of the UV cuvettes as this will invalidate your results.
Part 1: Preparation of a calibration curve
A calibration curve should be constructed using at least five concentrations of the pure paracetamol standard
supplied in the range 3-15 ug/mL as follows:
Weigh about 150 mg of paracetamol accurately and transfer to a 200 mL volumetric flask. Add 50 mL of o.1 M
NaOH and dilute to about 100 mL with deionised water (DI). Shake and make up to volume with DI water. Dilute
10 mL of the resulting solution to 100 mL (volumetric flask) with DI water (= stock solution). Prepare standard
solutions containing 3, 6, 9, 12 and 15…
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Related Questions
- read the Procedure and answer the post lab questions below: Using a balance, mass between 1.50 – 2.00 grams of sodium carbonate in a pre-massed 150mL beaker. Add 20 mL of distilled water and stir thoroughly to make sure all the crystals are dissolved. Rinse the stirring rod with a little distilled water after stirring. Using a balance, mass between 1.50 – 2.00 grams of calcium chloride dihydrate in a pre-massed 50 mL beaker. Repeat Step 2 for the solution in the 50 mL beaker. Pour the calcium chloride solution into the 150mL beaker containing the sodium carbonate solution and stir. Mass a piece of filter paper. Fold the filter paper and place it into the funnel. Wet it with a little distilled water to ensure that it is stuck to the sides of the funnel. Slowly pour the mixture from the beaker into the funnel and collect the filtrate into a 125mL erlenmeyer flask. Do not allow the mixture to rise above the edge of the filter paper. Rinse the beaker with about 10 mL of distilled water.…arrow_forwardread the Procedure and answer the post lab questions below: Using a balance, mass between 1.50 – 2.00 grams of sodium carbonate in a pre-massed 150mL beaker. Add 20 mL of distilled water and stir thoroughly to make sure all the crystals are dissolved. Rinse the stirring rod with a little distilled water after stirring. Using a balance, mass between 1.50 – 2.00 grams of calcium chloride dihydrate in a pre-massed 50 mL beaker. Repeat Step 2 for the solution in the 50 mL beaker. Pour the calcium chloride solution into the 150mL beaker containing the sodium carbonate solution and stir. Mass a piece of filter paper. Fold the filter paper and place it into the funnel. Wet it with a little distilled water to ensure that it is stuck to the sides of the funnel. Slowly pour the mixture from the beaker into the funnel and collect the filtrate into a 125mL erlenmeyer flask. Do not allow the mixture to rise above the edge of the filter paper. Rinse the beaker with about 10 mL of distilled water.…arrow_forwardColor BEFORE adding Color AFTER adding Intensity of color AFTER adding FeCl3 Test Tube # FeCl3 FeCl3 #1 (salicylic acid) clear lilac 100% #2 (commercial aspirin A) clear slightly pink 50% #3 (commercial aspirin B) clear lilac 95% #4 (aspirin from your clear pink 20% synthesis above) #5 (control) clear clear 0% Based on this data and the melting point of Aspirin, how pure is the synthesized product?arrow_forward
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SEE MORE QUESTIONS
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