Agarwood Oil Lab

Part 1: Esters aromas are very distinct and often pleasant, they are often used in food aroma and fragrances.1 Esters chemical properties are distinguished by their low molecular weight and low boiling points, caused by their dipole-dipole and dispersion interaction.2 Esters are the result of a condensation reaction, in which a carboxylic acid, an alcohol, and an acid catalyst react to create a water molecule and an ester.

Research Question: How does the size of the cell affect its efficiency in exchanging substances through several ways, like diffusion?

Abstract: One mixture of two unknown liquid compounds and one mixture of two unknown solid compounds were separated, isolated, purified, and characterized by boiling point. Two liquid unknowns were separated, isolated, and purified via simple distillation. Then, the process of an acid-base extraction and washing were used to separate two unknown compounds into two crude compounds: an organic acid and a neutral organic compound. Each crude compound was purified by recrystallization, resulting in a carboxylic acid (RCO2H) and a pure organic compound (RZ). The resulting mass of the pure carboxylic acid was 1.688g with a percent recovery of 31.80%, the boiling range was 244-245 °C, and its density was 2.0879g/mL. The resulting mass of the pure organic solid was 2.4902g with a percent recovery of 46.91%, the boiling range was 52.0-53.4°C, and its density was 1.5956 g/mL.

Answer: Gas chromatography (GC) – utilized by scientists in order to be able to separate the volatile

When looking over my results, I found that the pH level increased from a neutral pH to a basic level of pH. The Miracle- Gro fertilizer that I used is supposed to have a pH of 7. This surprised me because I would think that adding a 10% fertilizer solution would make the water acidic. I thought that the fertilizer would be more acidic because when we learned about rivers, we found out that acid rain decreased the dissolved oxygen levels; also, Eutriporication results in low dissolved oxygen levels. Therefore I believed that the fertilizer would be acidic because of my background knowledge of dissolved oxygen in water. Regardless, the basic water killed the algae, elodea plant and the snails in the water. I also thought that eutrophication would occur in the water when

In this lab, the molar mass of a volatile liquid is determined based on its physical properties in the vapor state. In order to calculate the molar mass, the mass, temperature, pressure, and volume is measured independently and then converted to the correct units. Sample C was obtained at the beginning of the experiment, which was later informed to be ethanol. Based on the calculations made, the molar mass of the volatile liquid was 95.9 g/mol. However, compared to the known value of 46.1 g of ethanol, the value measured had a 108% error. Unfortunately, this was a very big percent error and may have been caused by incorrectly measuring the volume of the gas. Using the ideal gas law, the molar mass of a volatile compound was calculated in order

The purpose of the lab was to synthesize aspirin and oil of wintergreen, and to determine its purity using recrystallization process, determining its melting point and using back-titration. To synthesize aspirin, salicylic acid and anhydride was used to drive the reaction to completion. In the synthesis of oil of wintergreen we reacted salicylic acid and methanol to produce methyl salicylate. This reaction is an example of a condensation reaction where the carboxylic acid and alcohol group combine to form an ester. In producing aspirin, we wanted to obtain the purest form, so we removed impurities such as unreacted salicylic acid and acetic acid. Acetic acid was removed by rinsing the sample in water because acetic acid is soluble in water. Salicylic, however, was removed by using the recrystallization process because it is insoluble in water. To recrystallize, we dissolved a sample of crude aspirin in warm ethanol and let it cool. Because aspirin is less soluble in ethanol than salicylic acid, it will crystallize out of the solution. To obtain the purified aspirin sample, we then filtered the solution to separate it from the impurities. To determine qualitatively the purity of the recrystallized aspirin, we determined its melting point using a melting point apparatus. Using the idea of freezing point depression, the presence of impurities will lower the melting point of the substance. Thus, by comparing the melting point to the actual

The purpose of this laboratory experiment was to isolate and characterize clove oil in order to understand how to isolate organic compounds with high boiling points, how to perform and interpret qualitative tests for organic compound functionality, and to continue to learn how to perform and interpret IR spectrometry. Steam distillation was used in order to prevent the organic compound from decomposing at temperatures approaching the compound's boiling point.

Purpose: The purpose of this experiment is to isolate the major component of anise oil and determine its identity and structure using melting point determination and IR spectroscopy.

The purpose of this experiment is to determine the molar mass of an unknown volatile organic liquid, using methods such as, the Dumas method, and then state its identity.

The objective of this experiment is to prepare and identify several types of esters by the process of dehydration synthesis using an alcohol with an acid.

The bottom of the cup is blackened and the water was emptied from the cup.

Dispense .5 mL water into the already weighed conical vial, replace cap and face insert on its down side.

Purpose: The purpose of the experiment was to perform the acid-catalyzed Fischer Esterification of acetic acid and isopentyl alcohol to form isopentyl acetate, or banana oil, which is used in flavor industries. The equilibrium of the reaction was changed by adding an excess amount of acetic acid. The reaction was refluxed and product was purified by extraction and distillation. Isopentyl acetate was analyzed by infrared spectroscopy and 1H NMR spectroscopy.

Each test performed in the lab on theses unknown bacteria have a very specific significance. With each test performed correctly the lab officer is able to move closer towards a proper identification of the unknown bacteria. After performing Gram staining and deciphering if the unknown was gram positive or negative the lab officer was then able to proceed to the next step of identification. The gram positive unknown’s reaction to the catalase test informs the tester of the Genus theyre working with. This indicates which tests to perform next. The MacConkey agar is a selective medium that only allows the growth of gram positive bacteria confirming the results received from the gram staining procedure. The NaCl growth test indicates whether or not the organism is able to