Procedure The powdered cobalt oxalate hydrate was weighed to about 0.3 g and placed in a pre-weighed crucible. The crucible and the cobalt oxalate were then heated until the cobalt oxalate decomposed into a stable, black solid, or Co3O4. Once the crucible was sufficiently
Procedure: Part 1: Obtain some 0.200M Fe(NO3)3 solution and some 0.00020M KSCN solution. Starting from the first solution, pour and mix 8.0mL of Fe(NO3)3 solution and 2.0mL of KSCN solution into a test tube, where as the second solution has 7.0mL of Fe(NO3)3 solution and 3.0mL of KSCN solution. Continue this process until 5 test tubes have been filled. Pour
Experiment 1: Synthesis and Recrystallization of Adipic Acid Aim The current experiment sought to prepare 1,6-hexanedioic acid (adipic acid) by catalytic oxidation of cyclohexene in the presence of a phase-transfer catalyst (Aliquat 336), using sodium tungstate as a catalyst and hydrogen peroxide as an oxidant. Introduction The carbon-carbon double bond of alkenes represents a
The experiment first started by the calculation of the net oxygen production under white light, it started by putting the Elodea in a volumeter tube containing 3% sodium bicarbonate solution, which was assembled to the volumeter by covering the tube with the plug/pipet/syringe assembly (a 1-2cm air space between the bicarbonate solution and the top rubber cover of the volumeter tube should be left.) Then, clamp the volumeter onto the clamp stand using the tube clamp and fill 2000ml beaker with cold tap water. The beaker should be placed on the clamp stand between the volumeter tube and the light lamp. A five minutes stabilization
Synthesis of Bromoacetanilide An ice bath was prepared in a large beaker and a small cotton ball was obtained. 0.5 g of acetanilide, 0.9 g of NaBr, 3mL of ethanol and 2.5 mL acetic acid was measured and gathered into 50mL beakers. In a fume hood, the measured amounts of acetanilide, NaBr, ethanol and acetic acid were mixed in a 25mL Erlenmeyer flask with a stir bar. The flask was plugged with the cotton ball and placed in an ice bath on top of a stir plate. The stir feature was turned on a medium speed. 7mL of bleach was obtained and was slowly added to the stirring flask in the ice bath. Once all the bleach was added, stirring continued for another 2 minutes and then the flask was removed from the ice bath and left to warm up to room temperature. 0.8mL of saturated sodium thiosulfate solution and 0.5mL of NaOH solution were collected in small beakers. The two solutions were added to the flask at room temperature. The flask was gently stirred. Vacuum filtration was used to remove the crude product. The product was weighed and a melting point was taken. The crude product was placed into a clean 25mL Erlenmeyer flask. A large beaker with 50/50 ethanol/water
Apparatus: • Bunsen or lab burner -Test tube clamp • Butane safety lighter - Test tube rack • Evaporating dish - Wash bottle • Forceps or crucible tongs - Wood Splints • Heat resistant pad • Litmus paper • Pipets • Spatula • Test tubes Materials: Ammonium carbonate, 0.5g Calcium carbonate, 0.5g Copper chloride solution, 4mL Hydrochloric acid, 4mL Magnesium ribbon, 2-4 cm strips Phenolphthalein indicator, 1 drop Sodium hydroxide solution, 1mL Sodium phosphate solution, 1mL Water 28. Record the observations in the data table. Reaction 8) 29. Working in the hood or a designated work area, add about 1 mL of ethyl alcohol to a clean evaporating dish. Place the evaporating dish on a heat- resistant pad.
14 mL of 9 M H2SO4 was added to the separatory funnel and the mixture was shaken. The layers were given a small amount of time to separate. The remaining n-butyl alcohol was extracted by the H2SO4 solution therefore, there was only one organic top layer. The lower aqueous layer was drained and discarded. 14 mL of H2O was added to the separatory funnel. A stopper was placed on the separatory funnel and it was shaken while being vented occasionally. The layers separated and the lower layer which contained the n-butyl bromide was drained into a smaller beaker. The aqueous layer was then discarded after ensuring that the correct layer had been saved by completing the "water drop test" (adding a drop of water to the drained liquid and if the water dissolves, it confirms that it is an aqueous layer). The alkyl halide was then returned to the separatory funnel. 14 mL of saturated aqeous sodium bicarbonate was added a little at a time while the separatory funnel was being swirled. A stopper was placed on the funnel and it was shaken for 1 minute while being vented frequently to relieve any pressure that was being produced. The lower alkyl halide layer was drained into a dry Erlenmeyer flask and 1.0 g of anhydrous calcium chloride was added to dry the solution. A stopper was placed on the Erlenmeyer flask and the contents were swirled until the liquid was clear. For the distillation
Methylcyclohexene Ashton Krstevski Lab Partner: Micheal O’Daniel Organic Chemistry 1 Laboratory, Indiana University Northwest, Gary, Indiana 46408 October 28, 2016 Abstract: The purpose of this experiment was to practice the functional group transformation procedure. The process of the experiment included the dehydration of 2-methylcyclohexanol in the presence of phosphoric acid and heat. The products that were
VO3− + 4H+ + e− →VO2+ +2H2O (1) Experimental Procedure Reduction of VO3- Seven test tubes were labeled numerically with 2 mL of VO3- and H2SO42- added to each tube. A small pea size portion of solid Na2SO3 was added to the first test tube. Then, 20 drops of distilled water were added to the second test tube. In the third test tube, 20 drops of (.2 M) NaBr were added. Then, to drops of (.2 M) NaNO2 were added into the fourth test tube. A small portion of Fe(NH4)2(SO4)2 * 6H2O was added into the fifth test tube. The sixth test tube had 20 drops of (.2 M) H2Cr2O4 added, where the seventh test tube was the control tube with no additional chemicals added. All the test tubes were left to react for 3 minutes and then heated in a heated bath for approximately 20 minutes.
The crude product was washed by taking the reaction product in the separatory funnel and adding 23 mL of deionized H2O. The mixture was shaken and allowed to settle until layers were observable. The top layer was the desired product and approximately 25 mL of aqueous layer was extracted from the separatory funnel. Next, 25 mL of 5% NaHCO3 was added to the separatory funnel in order to neutralize the acid. This mixture was swirled, plugged with the stopper and inverted. Built-up gas was released by turning the stopcock to its opened and closed positions, releasing CO2 by-product. This was done four times in one minute intervals. The solution was allowed to settle until layers were observable. The bottom layer that contained salt, base and water was extracted from the separatory funnel. The crude product was washed again as mentioned previously.
Logic Homework 1.1: I 1. a. P) Carbon monoxide molecules happen to be just the right size and shape, and happen to have just the right chemical properties, to fit neatly into cavities within hemoglobin molecules in blood that are normally reserved for oxygen molecules.
Haemoglobin is a protein molecule found in red blood cells (RBC). Its role in the body is to transport oxygen from the lungs to the body 's tissues and then returns carbon dioxide from the tissues back to the lungs. The transportation of oxygen is only possible when haemoglobin (Hb) within the RBC binds to oxygen. (Martini & Nath, 2006)
The soda ash form experiment 3 was obtained. A 250 ml beaker was obtained and rinsed.
Funny; there is a predisposed notion among my colleague about how scientific research could be very daunting. But, luckily, this project was everything but daunting; In fact, it was intriguing! Indeed! That was how I felt when my academic research pertaining to the 27th element, Cobalt, led me to discovery the following: That the element was discovered 281 years ago to this year, in Sweden in 1735, by chemist George Brand (Thomas); Brand, fascinated by the idea that the blue color of glass and orbs found in mines could not be caused by the element Bismuth, officially named Cobalt as the element that was responsible to have caused the blue color seen on glasses and orbs after conducting his own experiment (Thomas). Unfortunately, that was all
������ Equipment, Materials, and Method The equipment used were a jacketed batch reactor beaker, cooling water circulation system, computer, LabPro temperature probe and conductivity probe, mixing stand and magnetic stir bar. The materials used for this reaction were a 0.08M NaOH solution and a 0.1M ethyl acetate solution. A 20% excess Ethyl acetate was used to ensure NaOH was the limiting reactant.[1] NaOH was chosen for the limiting reactant because of its high conductivity relative to Ethyl acetate. The extent of the reaction was monitored by measuring the conductivity throughout the reaction. With NaOH being the limiting reactant, the change in conductivity is more visible, and the termination of the reaction can