Composition And Molecular Formula Of An Inorganic Double Salt

In the hood, place the copper wire in 10mL of nitric acid and wait for it to dissolve. Afterwards, add 100mL of deionized water to the solution and boil the solution, so all the nitrogen oxides are removed. Place the solution to a 250.0mL volumetric flask and add deionized water to the flask until the solution is 250.0mL. When the solution in the flask is at 250.0mL place the solution in a clean plastic bottle. Now cut a penny into four pieces, and measure the mass of all the pieces together. Go back to the hood, and place the pieces of the penny into a 250mL beaker. Afterwards, add 20mL of concentrated hydrochloric acid. Wait for the hydrochloric acid to dissolve the zinc core. When the zinc has dissolved, filter the solution through the filter paper, and place the copper metal pieces into a clean 150mL beaker. In the hood, place 4mL of concentrated nitric acid in the beaker, and when the copper dissolves add, one drop at a time, 30mL of 6 M ammonium hydroxide to neutralize the nitric acid. Transfer the copper/ammonia solution to a 100.00mL volumetric flask. Prepare four different calibration

To prepare the penny samples three pennies were obtained with one penny assigned to each group member. Each penny was weighed and their masses were recorded in the notebook. The year the pennies were made and the condition the pennies were in were also recorded in the notebook. In the fume hood each penny was placed into a 150 mL beaker. 25 mL of 6 M HNO3 was added to each beaker. The pennies dissolved and the remaining solutions were left to cool for 10 minutes. The three beakers’ contents were quantitatively transferred into three separate 100 mL volumetric flasks using a funnel. To make sure there was no loss of sample, the beaker was rinsed with 5-10 mL of water four times, each time the rinse solution being added to the volumetric flask. Still in the fume hood, 14 mL of concentrated ammonia solution was added to each volumetric flask using a graduated cylinder. The volumetric flasks were swirled to establish the blue color and dissolve any solids. If any

This experiment is based on determining the chemical formula for a hydrated compound containing copper, chloride, and water molecules in the crystal structure of the solid compound, using law of definite proportion. The general formula of the compound is CuxCly•zH2O, and aim is to determine chemical formula of this compound.

In this task the concentration of an unknown sample of copper sulphate using colorimetry was used to find the concentration. In this investigation copper sulphate was used which is CuSO4.5H20 as a formula. To make a standard solution which was 1M, the same clean equipment was used to make up the standard solution as used to make sodium carbonate. However there was one difference and that was that the hot distilled water was used to dissolve the copper sulphate crystals. There had to be enough hot water in order to dissolve the crystals into the beaker and then add cold distilled water to cool the solution.

When the red Co(NO3)2*6H2O crystal was added to the white NH4 crystal, and water was added to dissolve, the solution turned blue in color. As the solution was nixed, the color changed to that of a blue-purple and a blue precipitate formed. When the 6 M NH3 began to be added, the color shifted to dark purple color after 15 mL of ammonia and the amount of the precipitate was less. After 20 mL of ammonia, the solution became a red brown with very little of the blue precipitate. After 30 mL of ammonia, the solution was similar in color to an iodine solution, a dark brown-red, almost black in color. At this point there was no visible precipitate on the surface of the solution. After 40 mL of the ammonia had been added, the solution was the same iodine like color as before. When closely examined, there was a black precipitate that had settled on the bottom of the beaker. At this point, hydrogen peroxide, 3% H2O2, was added to solution. After 4 mL of the H2O2 was added, the solution was the same color and the precipitate had not changes. After 8 mL of the H2O2, there was not noticeable change. After 12 mL of the H2O2, the solution was slightly redder in color but the precipitate had not changed. After 15 mL of H2O2, the solution was the same color and no changes had occurred to the precipitate. At 17 mL, the solution began to effervesce slightly, though there

Then 8.0g of copper sulfate crystals were placed inside the beaker and the mass was recorded for the actual crystals. 50 mL of water was added to the beaker with the crystals. The ring stand was set up with the wire mesh on it and one partner should place the mixture in the beaker on it should be heated without letting the mixture boil. Stir the mixture and heat until the crystals are dissolved. While one partner does this, the other should obtain 1.5g of iron filings in a measuring cup and records the mass. Then the iron filings should be added small amounts at a time to the heated solution. Stir continuously until all the mixture is added to the beaker. Then it sat for 10 minutes and observations were recorded. Record the mass of a filter paper and set up a filtration apparatus with the filter paper in a funnel over an Erlenmeyer flask. Decant the liquid through the paper slowly trying not to allow any solid to get on the filter paper. Then with de-ionized water, rinse your solid in the beaker and let the solid settle then decant the liquid. Repeat the washing twice more and in the last time guide all the solid into the filter paper. Then place the filter paper on a watch glass and then into a warm oven to dry. After it is cool, record the mass of the watch glass, filter paper and solid. If there is not enough time to cool, you may have to do it the next

B2.Place a few crystals of copper(II)sulfate pentahydrate in a test tube. Clamp the tube and heat in a horizontal position. One of the products is copper(II)sulfate. What is the other one? This decomposition reaction is easily reversible. Add a dropperful of water to the tube when it cools. Record what happens.

Part 1: Obtain some 0.200M Fe(NO3)3 solution and some 0.00020M KSCN solution. Starting from the first solution, pour and mix 8.0mL of Fe(NO3)3 solution and 2.0mL of KSCN solution into a test tube, where as the second solution has 7.0mL of Fe(NO3)3 solution and 3.0mL of KSCN solution. Continue this process until 5 test tubes have been filled. Pour

The purpose of this lab was to determine the percent cobalt and oxalate by mass, and with that information, the empirical formula for cobalt oxalate hydrate, using the general formula Coa(C2O4)b.cH2O.

During the heating period, a noticeable change took place in the sugar test tube – it began to caramelize, melting into a golden brown color, then finally a dark brownish/black hue; it remained constant at that color. The copper sulfate began losing color when applied to the heat, turning from a bright blue to white and remained white after heating. Once cooled, 2-3 drops of water were added to each tube; the sugar remained the same, while the copper sulfate immediately bubbled and transformed from white back to its original blue hue. Next 1-3 grams of the hydrated copper sulfate were added to a crucible, which was weighed prior to adding the sample, then heated gently with a Bunsen burner. Once the salt stopped changing color, it was heated for an additional 5 minutes, then the total mass was measured. Finally, a pea-sized amount of Epsom Salt was added to a test tube and heated for 1 minute without the tube becoming red

Seven test tubes were labeled numerically with 2 mL of VO3- and H2SO42- added to each tube. A small pea size portion of solid Na2SO3 was added to the first test tube. Then, 20 drops of distilled water were added to the second test tube. In the third test tube, 20 drops of (.2 M) NaBr were added. Then, to drops of (.2 M) NaNO2 were added into the fourth test tube. A small portion of Fe(NH4)2(SO4)2 * 6H2O was added into the fifth test tube. The sixth test tube had 20 drops of (.2 M) H2Cr2O4 added, where the seventh test tube was the control tube with no additional chemicals added. All the test tubes were left to react for 3 minutes and then heated in a heated bath for approximately 20 minutes.

40 g of ice and approximately 30 ml of sulfuric acid is cautiously added to a 100 mL beaker respectively. Weigh 7.6 g of ammonium chloride and 14.0 g of ammonium bromide and place it in another beaker, crushing the lumps until a powdery mixture remains. The powdery mixture is then transferred to a 125 mL Erlenmeyer flask. Add the ammonium salts into the sulfuric acid mixture. Heat is applied to dissolve the salt. Once the

In this experiment, a saturated calcium sulfate was already made and ready to use. 25.00 mL of this solution was then mixed with 10 mL of an ammonia buffer and 1 drop of

2cm of a solution was tested and added 2 cm of 10% of potassium hydroxide solution and the test tube was shaked.

At the end of the experiment when the lid was removed, it was found out that the blue colour of the copper (II) sulphate solution has faded away. It was turned to pale grey and there were some precipitates present. It was the zinc powder that was in excess to ensure that the copper (II) sulphate solution could react fully with the zinc powder.