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Erlenmeyer Lab Report

Satisfactory Essays

For safety concerns, the titrant was handled with gloves when pouring. and eyeglasses were worn to prevent liquid from entering it. In addition, hair was tied back and enclosed shoes were worn during the experiment. The procedure is as follows: 1. There were 3 Erlenmeyer flasks, one burette and burette clamp, a ring stand, and weighing paper placed on one side of the work station. 30ml of deionized water was placed in an each of the three Erlenmeyer flasks. 2. Two 1.033 and 1.041 grams of analyte were weighed and placed on the electronic balance with weighing paper and poured into the Erlenmeyer flasks. After the analyte was added, 15 ml of 3 M H2SO4 was added also. 3. The glass rod was rinsed with deionized water and the 15 ml of 3 M H2SO4 was swirled into it …show more content…

The burette was placed in the burette clamps on the ring stand in filled with 0.050 M KMnO4 solution till the 0.00 ml. 5. The Erlenmeyer flask was placed on the ring stand and KMnO4 was added and stirred until a light pink color was reached. The initial and final volume of the KMnO4 was recorded with the initial volume always starting at 0.00 ml. Steps 4-5 was repeated and recorded two more times for the initial and final volume of the two remaining flasks. 6. All materials were rinsed, except burette clamp, a ring stand, safety goggles, an electronic balance, and weighing paper with deionized water and set on a paper towel. 7. The initial and final volume along with the grams of the analyte was recorded on the data sheet and the amount of KMnO4 for each flask was calculated. Calculations and recordings of the mass percent of iron in the unknowns were finished. Observations/Data: The following observations were observed doing the experiment. The KMnO4 was a deep purple and when ~ 5ml of KMnO4 was added to the colorless solution it turned faintly pink. Furthermore, when adding the anaylate to the acidic solution, it dissolved after about ~50 (s) of swirling the solution in an Erlenmeyer

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