Kalah Bailey October10th 2015 Chem 109 Pre-Lab 6 Title: Observations of Chemical Reactions. In this lab, students will recognize and record the chemical reaction results of seven different anions and one cation. This experiment also focuses on the reaction of salt solutions and what happens when two different solutions mix. Procedure: • Carbonate (CO32-) - First, solid calcium carbonate (CaCO3) is added to a test tube in a small amount. Next, 15 to 20 drops of 6M HCl are placed in the tube. The result is then recorded. - 15 to 20 drops of 1M Na2CO3 are poured in a separate test tube. Then 15 to 20 drops of 6M HCl are slowly added to the tube and the outcome is recorded. • Sulfate (SO42-) -Second, in a test tube 15 to 20 drops of 0.1 Na2SO4 are added. 5 drops of 0.5M BaCl2 are placed in the tube and the solution is stirred. The result is recorded. • …show more content…
Next, 1to 2 drops of 6M HNO3 and 5 drops of 0.1M AgNO3 are added and the solution is stirred. The observation is recorded. - In the same tube, 6M NH3 is transferred drop after drop and is stirred until a change happens. The reaction is then recorded. • Iodide (I-) -Fourth, 15 to 20 drops of 0.1M KI are moved into a test tube. A small amount of AgNO3 is added and the result is recorded. - In the same tube, 20 drops of 6M NH3 is placed drop after drop and is stirred. The observation is recorded. • Acetate (C2H3O2) -Fifth, 15 to 20 drops of 1M NaC2H3O2 are added to a test tube followed by15 to 20 drops of 3M H2SO4. The solution is stirred and any odor is distinguished. Then, the outcome is
Solutions of 6M H2SO4, 6M NH3, 6M HCl, 6M NaOH, and 1.0 M of NaCl, 1M Fe(NO3)3, 1M NiSO4, 1M AgNO3, 1M KSCN, 1M Ba(NO3)2, and 1M Cu(NO3)2 were given in separate test tubes. The color of possible precipitates, ions, acid-base behaviour, odor and solubility rules were conducted and were reported in Table 1. The key information about a mixture of two solutions was
The crude product was washed by taking the reaction product in the separatory funnel and adding 23 mL of deionized H2O. The mixture was shaken and allowed to settle until layers were observable. The top layer was the desired product and approximately 25 mL of aqueous layer was extracted from the separatory funnel. Next, 25 mL of 5% NaHCO3 was added to the separatory funnel in order to neutralize the acid. This mixture was swirled, plugged with the stopper and inverted. Built-up gas was released by turning the stopcock to its opened and closed positions, releasing CO2 by-product. This was done four times in one minute intervals. The solution was allowed to settle until layers were observable. The bottom layer that contained salt, base and water was extracted from the separatory funnel. The crude product was washed again as mentioned previously.
You find a sample of a solution that has a faint odor resembling vinegar. You are verifying that it is indeed vinegar and you add a few drops of phenolphthalein. The sample turns pink. What assumptions can you make about this sample?
The objective of the experiment was to observe different reactions with different chemicals. The experiments emphasized on the chemical changes occurring in acids and bases as well as color changes and bubble formations. The experiments allowed for a better understanding of the undergoing chemical changes in mixtures. Some mixtures instantly changed colors while others were transparent or foggy. Some mixtures produced thick color that created solids called precipitates. Mixtures KI + Pb(NO3)2 and NaOH + AgNO3 both produce noticeable precipitates after a while. It was interesting to see the different acidic and base reactions like the fuchsia color formation in NaOH + phenolphthalein.
An automatic pipet was used to measure 0.450 mL water and 0.165 mL acetic anhydride and was added to the conical vial. A spin vane was placed into the vial and an air condenser was attached.
In reference to the analysis of anions, Table 1 shows that a precipitate was formed when our unknown was combined with HNO3 and AgNO3, thus indicating the presence of a chloride ion. Because our unknown did not form a precipitate due to HCl and BaCl2, separate, effervesce, or smell, we concluded that neither sulfate, nitrate, carbonate nor
ii. The second part of the titration series involves titration of NaOH with Hydrochloric acid (HCL). Again, three reps of titration and a blank titration have to be completed. A volumetric pipet is used to measure 10.00mL of HCL into three labeled conical flasks. Then the flasks are filled with deionized water until about the 50mL mark. A buret is
The main objective of this experiment is to differentiate between a physical change and a chemical change.
Dispense .5 mL water into the already weighed conical vial, replace cap and face insert on its down side.
8. Repeat step 7 with H2SO4, except that you should use a 10 mL graduated cylinder of H2SO4 and adding 15 mL water.
In this experiment, a saturated calcium sulfate was already made and ready to use. 25.00 mL of this solution was then mixed with 10 mL of an ammonia buffer and 1 drop of
* By using the dropper and measuring cylinder, 7 ml sodium carbonate solution was added to the test tube
These reactions can be seen from just a little bit of reaction all the way up to a complete change of the entire sample tested. Some samples of those tested in this experiment which showed the chemical reaction were the baking soda/ammonia mixture, the Epson salt and baking soda mixture as well as the food coloring mixed with the baking soda and bleach. 2. Which reactions, if any, do you believe showed no evidence of chemical change? Justify your reasoning.
The purpose of this lab is to test substances and to determine the physical and chemical properties of substances.
Sodium hydrogen carbonate was added to the solution until it becomes neutral. Ph paper was used for this test to determine its ph value.