Oxidation – Reduction Titration: Determination of Iron (II) Essay

The primary goal of this laboratory is to correctly identify an unknown substance. To achieve this task, one may use various tests that reveal both chemical and physical properties of a substance. By comparing the results of a known substance and the unknown substance, one may eliminate alternative possibilities and more accurately predict the undisclosed compound. Furthermore, by performing these tests, data can be collected and verified regarding chemical and physical properties of the unknown. Understanding the chemical properties of a known substance aids one’s understanding of the unknown based on comparative analysis of the results of the tests.

Washing of the copper is necessary in this experiment to separate the iron from the copper and make sure the iron is not counted in the mass of the copper.

Experimental Method: A filtration apparatus was set up. Solid iron(III) chloride hexahydrate was dissolved in water. In a separate container, sodium acetate trihydrate (NaC2H3O2 x 3 H2O) was also dissolved in water. Sodium acetate trihydrate was then added to iron(III) chloride. 2, 4-pentanedione (C5H8O2) was dissolved in methanol; it was then added to the iron(III) chloride/sodium acetate solution. The product of this mixture was filtered, and the precipitate

Enter the precise mass in GRAMS of the potassium iodate used to prepare your primary standard solution.

The purpose of this lab was to determine the limiting reactant in a reaction between copper sulfate and iron. Using the reaction between copper sulfate and iron, the reaction was observed to see the reaction and transformation of matter. The copper sulfate was placed into a beaker, as the excess reactant, then iron filings added until the heated solution was completely reacted. This reaction created an excess of leftover. The law of conservation of mass can be observed in this reaction, and using the data found, the percent yield calculated.

• Determine concentration of enzyme stock solution, if unknown, by taking an A280 nm reading of a 1:100 dilution (in water). Use a total volume of 1 ml in the cuvette.

0.1 gram of my product from the second trial was weighed in a tray and was then added to a fourth test tube containing 2.0 mL of Iron (III) chloride, which was measured using a 10 mL graduated cylinder, to test for

Part 1: Obtain some 0.200M Fe(NO3)3 solution and some 0.00020M KSCN solution. Starting from the first solution, pour and mix 8.0mL of Fe(NO3)3 solution and 2.0mL of KSCN solution into a test tube, where as the second solution has 7.0mL of Fe(NO3)3 solution and 3.0mL of KSCN solution. Continue this process until 5 test tubes have been filled. Pour

Begin by labeling two sets of 7 different 1.5 ml tubes 0 thru 6. Obtain 1 more 1.5 ml tube and label it B for the blank. Obtain 1 sample of 15 μls from each of the serially di-luted tube concentrations and put it in its corresponding 1.5 ml tube. Now add 525 μl of media in each 1.5 ml tube, followed by 60μl of Alamar Blue in each tube. Close the lids of all the tubes and vortex for 5 seconds. In order to make the blank, add 180 μl of media and 20 μl of Alamar Blue in another 1.5ml tube.

b) Iron and Barium were present in unknown 3. Assigned unknown reacted with all 4 reactants and formed precipitate with 3 of them (Sodium carbonate, sodium hydroxide and Sulfuric acid). During the experiment it reacted very similarly to Iron (III) nitrate and Barium nitrate. For example, with it was tested against Ammonium Chloride, the color of the solution changed to a light green, very identically to Iron (III) nitrate and Ammonium Chloride. Besides, unknown 3 formed an orange brownish precipitate when it was tested with sodium carbonate. Iron (III) nitrate acted similarly. Moreover, unknown 3 reacted similar to Barium nitrate when it was tested against ammonium chloride and sulfuric acid. It did not form any precipitate with ammonium chloride but formed a very light white precipitate, which is identical to barium nitrate’s reaction against sulfuric acid. Therefore, the two present metal in unknown 3 are Iron and barium.

Iron is one of the important minerals that is required for our bodies to function properly. Most of the iron in our body is found in the blood such as haemoglobin, approximately 60 -70% of the human body’s iron is found in the haemoglobin, a protein in the blood that transports oxygen. Iron is also present in muscle tissue and some enzymes. There are two types of iron in the body which are “Heme Iron” from animal products and “Non-Heme Iron” vegetables and

The first reaction involves pyrite rock reacting with oxygen (air) and water to produce dissolved ferrous iron, sulfate, and acidity. The second reaction oxidizes the dissolved ferrous iron in acidic conditions and produces ferric iron and water. The third reaction involves the hydrolysis of the ferric iron to form ferric hydroxide and more acid. The ferric hydroxide is the orangey-red colored solid you see in the water (Juniata College).

Refer to the reaction of iron nails with a copper solution assignment in Module 3, Section assignment 3.4 Part F of the Chemistry 11 course.

The lab performed required the use of quantitative and analytical analysis along with limiting reagent analysis. The reaction of Copper (II) Sulfate, CuSO4, mass of 7.0015g with 2.0095g Fe or iron powder produced a solid precipitate of copper while the solution remained the blue color. Through this the appropriate reaction had to be determined out of the two possibilities. Through the use of a vacuum filtration system the mass of Cu was found to be 2.1726g which meant that through limiting reagent analysis Fe was determined to be the limiting reagent and the chemical reaction was determined to be as following:-

Using Graph 1: The Volume of Titrant Added in order to reach the Endpoint and the Corresponding pH Values, observe the vertical line of each titration and see the points in which the horizontal lines intersect it. These points give the