Essay about Qualitative Analysis Discussion

To determine which ions are present in the two unknown solutions. This will be accomplished by mixing three known solutions with three testing solutions. You will use this information to determine which ions are present in the unknown solutions.

The Copper Chloride displayed and used to complete this lab had led us to the following observations;

In this task the concentration of an unknown sample of copper sulphate using colorimetry was used to find the concentration. In this investigation copper sulphate was used which is CuSO4.5H20 as a formula. To make a standard solution which was 1M, the same clean equipment was used to make up the standard solution as used to make sodium carbonate. However there was one difference and that was that the hot distilled water was used to dissolve the copper sulphate crystals. There had to be enough hot water in order to dissolve the crystals into the beaker and then add cold distilled water to cool the solution.

to the unknown solution in order to completely precipitate the cations in part A. 2 A compound

In reference to the analysis of anions, Table 1 shows that a precipitate was formed when our unknown was combined with HNO3 and AgNO3, thus indicating the presence of a chloride ion. Because our unknown did not form a precipitate due to HCl and BaCl2, separate, effervesce, or smell, we concluded that neither sulfate, nitrate, carbonate nor

One of the most important skills to have in the chemistry lab is the understanding of how chemicals will react. Knowing for example, how a chemical will react with a metal, is an excellent way of determining the amount of a particular metal in a deposit. This knowledge was used in this lab to determine the amount of copper in an unknown sample mixture. It is also known that the determination of the percent concentration of a certain solution, will directly effect the percent transmission and absorption of a solution, dependent upon its dilution. By first testing known concentrations of a solution, and plotting this information graphically, a line is formed

The problem that was trying to be solved in this study deals with analyzing unknown solutions. In this particular case, a chemical company has several unknown solutions and to correctly dispose of them they need to know their properties. To figure out the properties several qualitative tests were performed throughout the study (Cooper 2012).

Pour 50 mL of distilled water into a 100 mL beaker, and then add the unknown substance into it. Mix thoroughly to create the aqueous solution. Now fill a new cuvette with this new solution and place into the SpectroVis Plus device; after wiping the outside with a Kimwipe as usual. Be sure to take note of the absorbance when wavelength is at its maximum. Afterwards, Be sure to take all solutions containing Iron(III) and pour them into the container specified for hazardous wastes. ​

the ions of SO42-, CO32-, Cl-, and I-,identify them separately, and use the observation to identify the unknown.

In well 3A there was a chemical reaction between the sodium phosphate and copper sulfate. There was a light blue precipitate formation which proves there was a chemical reaction.

An unknown material can be determined by using simple chemical tests and separations which is called as inorganic qualitative analysis. The separation of cations depends on the difference in their propensity to form precipitates. Separation scheme is used to classify cation into five groups on the basis of their physical and chemical behavior opposed to some reagents. Classification is based on whether there is formation of precipitates or not when metal cations react with the reagent. The five groups of cations and the characteristics of these groups are as follows:

The cations in both the known and unknown samples were identified by using qualitative analysis, of which were determined to be acidic, basic, or neutral by using litmus paper. Acid-base reactions, oxidation-reduction reactions, and the formation of complex ions are often used in a systematic way for either separating ions or for determining the presence of specific ions. When white precipitate formed after adding hydroxide, aluminum ion was determined to be present in the solution. However, nickel was determined to test positive when the solution changed to a hot pink color after adding a few drops of dimethylglyoxime reagent and iron was present when the solution was a reddish brown color when sodium hydroxide was added to the mixture at the very beginning of the experiment. Qualitative analysis determines that ions will undergo specific chemical reactions with certain reagents to yield observable products to detect the presence of specific ions in an aqueous solution where precipitation reactions play a major role. The qualitative analysis of ions in a mixture must add reagents that exploit the more general properties of ions to separate major groups of ions, separate major groups into subgroups with reactions that will distinguish less general properties, and add reagents that will specifically confirm the presence of individual

When the zinc was added to the copper (II) sulfate solution, the solution started to bubble. As the solution was stirred, it turned a cloudy blue. Small flecks of a brown solid were visible. As the solution became colorless, the brown solid settled to the bottom of the beaker. The solid formed was copper in its elemental state. The color faded from the solution as the copper ions slowly formed into solid copper. The copper was poured into a funnel with filter paper and washed three times with 25 mL

At the end of the experiment when the lid was removed, it was found out that the blue colour of the copper (II) sulphate solution has faded away. It was turned to pale grey and there were some precipitates present. It was the zinc powder that was in excess to ensure that the copper (II) sulphate solution could react fully with the zinc powder.

For generating valuable data with a desired accuracy and to quantify concentration of the constituents present in the samples being analyzed.