Spearmint and Caraway Oils: (+) and (-) Carvones Essay

Perform the following with three 0.05g samples of unknown and the following solvents: methanol, water and toluene

The distillation that was more efficient at separating the two compounds was the cyclohexane and the p-xylene since the curve of the graph for temperature vs. volume has a slightly better curve (Table 4A). The graph for cyclohexane and toluene was more linear (Table 4B). Furthermore, the mole fraction of cyclohexane and p-xylene was higher than the mole fraction of cyclohexane and toluene. For instance, the mole fraction of cyclohexane and p-xylene (when adding the mole fraction of the first ml and the last couple of drops) was 0.6604 while the mole fraction for cyclohexane and toluene was 0.13396. A higher mole fraction means that the compounds were purer which means that they separated better—since increasing the mole fraction increases the vapor pressure. Therefore, my hypothesis was supported.

Abstract: One mixture of two unknown liquid compounds and one mixture of two unknown solid compounds were separated, isolated, purified, and characterized by boiling point. Two liquid unknowns were separated, isolated, and purified via simple distillation. Then, the process of an acid-base extraction and washing were used to separate two unknown compounds into two crude compounds: an organic acid and a neutral organic compound. Each crude compound was purified by recrystallization, resulting in a carboxylic acid (RCO2H) and a pure organic compound (RZ). The resulting mass of the pure carboxylic acid was 1.688g with a percent recovery of 31.80%, the boiling range was 244-245 °C, and its density was 2.0879g/mL. The resulting mass of the pure organic solid was 2.4902g with a percent recovery of 46.91%, the boiling range was 52.0-53.4°C, and its density was 1.5956 g/mL.

B. Claim: As we go from 1-butanol  sec-butanol  1-ter-butanol the dipole moments and the surface areas decrease. As we go from 1-butanol  sec-butanol  1-ter-butanol the steric hindrance increases. As we go from 1-butanol  sec-butanol  1-ter-butanol the ΔT (degree of evaporative cooling) decreases. As we go from 1-butanol  sec-butanol  1-ter-butanol the strength of the IMFs decrease.

This experiment was done in order to understand both fractional distillations and gas chromatography. In addition, this experiment was done to separate and identify two liquids that made up an unknown mixture. Gas chromatography was used to figure out the ratio of these two liquids.

The purpose of this lab is to separate a mixture and determine the percentages of each of the ingredients. Each substance will have a different boiling point due to its intrinsic properties and from that, we will be able to determine the purity of different products as we evaporate off the next level of product.

The first step in extracting and analyzing the carvone from the spearmint oil was the column chromatography. The result of this was 1.88 grams of carvone product. The percent yield for this was 66.9% which indicates that a majority of the carvone was saved. This value is could have been decreased during the boiling off of the hexane. Some of the carvone product could have been evaporated if the water became too hot.

The purpose of this laboratory experiment was to isolate and characterize clove oil in order to understand how to isolate organic compounds with high boiling points, how to perform and interpret qualitative tests for organic compound functionality, and to continue to learn how to perform and interpret IR spectrometry. Steam distillation was used in order to prevent the organic compound from decomposing at temperatures approaching the compound's boiling point.

Objective: The objective of this experiment is to use acid-base extraction techniques to separate a mixture of organic compounds based on acidity and/or basicity. After the three compounds are separated we will recover them into their salt forms and then purify them by recrystallization and identify them by their melting points.

Name CHE 173 Sec # January 25, 2005 Experiment 36: Determination of the Structure of a Natural Product in Anise Oil

If the solutions are not mixed incorrectly then the results will come out the same way. The purpose of this study is to show the effects of tonicity with

The applications of this lab in real life would be being able to determinate the viscosity of fluids flowing through pipes, and also the net force acting on a spherical object flowing through those pipes due to the

1.) Briefly explain the concept of steam distillation. What is the difference between a simple distillation and a steam distillation? When a mixture of two immiscible liquids are distilled it is referred to as codistillation. This process is referred to as steam distillation when one of the liquids is water. This distillation is used to separate organic liquids from natural products and reaction mixtures in which the final product results in high boiling residues such as tars, inorganic salts, and other relatively involatile components. It is useful in isolating volatile oils from various parts of plants and not useful in the final purification of a

The purity and identity of the product can be determined through the use of smell, IR spectroscopy and melting point determination. A general idea of what the ester is can be obtained by smell. Esters can have specific smells and if the scent can be determined, one may have an idea of the ester was created. IR spectroscopy will identify the bonds of the functional groups. The ester can be considered pure if there are no additional peaks on the IR spectrum. For example, if a peak corresponding to an alcohol group appeared on the IR spectrum it would mean the ester is not completely pure. Melting point can also be used to confirm the identity and how pure the final product is. Comparison of the experimental melting point and the literature value allows for determination of how close the experimental value is to the literature value. If the experimental value is within the range of the literature value, the product can be considered pure.

concentration, record the absorbance readings at a fixed wavelength, and plot the absorbance vs. concentration data. The wavelength of 520 nm was selected for experiment Part