Synthesis of Co(Acac)3

In six different 50mL volumetric flasks there was 0.00 mL, 2.00 mL, 4.00 mL, 6.00 mL, 8.00 mL, and 10.00mL of the 5.00 g/L Cu^(2+)stock solution. 3mL of 15M ammonia was added into each flask, once the ammonia was added each flask was diluted with water to 50 mL then were all thoroughly mixed.

In this experiment an elemental copper was cycled a series of five reactions where it ended with pure elemental copper as well, but at different stages of the cycle the copper was in different forms. In the first reaction, elemental copper was reacted with concentrated nitric acid where copper changed the form from solid to aqueous. Second reaction then converted the aqueous Cu2+ into the solid copper II hydroxide (Cu(OH)2) through reaction with sodium hydroxide. The third reaction takes advantage of the fact that Cu(OH)2 is thermally unstable. When heated, Cu(OH)2 decomposes (breaks down into smaller substances) into copper II oxide and water. When the solid CuO is reacted with sulfuric acid, the copper is returned to solution as an ion (Cu2+). The cycle of reactions is completed with the

b. Using the newsvendor model, Cu = 1 - 0.2 = 0.8 and Co = .2. Cu /(Cu + Co) = .8.

The compound aquapentaamminecobalt(III) Nitrate, [Co(NH3)5OH2] NO3, is a metal complex bonded to the molecule nitrate to attain a neutral charge. The synthesis of this molecule is a more complex one, requiring the recrystallization of an intermediate species. When the complex has been formed and isolated via filtration, the complex can be reacted with various aqueous solutions, one being dimethyl sulfoxide, C2H6OS. When reacted these reagents form the compound Co(NH3)5(OS(CH3)2)3+, H2O, and NO3-, though not inn this ratio. Specifically the aquapentaamminecobalt(III) molecule can be used to study the sixth coordination site on the molecule where the later is bound. Because of the weaker bond between the cobalt ion and the water

The Cu Later lab experiment is designed to allow you to practice lab skills in implementing and performing a series of reactions. Specifically, four types of chemical reactions will occur: oxidation/reduction; double replacement; single replacement; and decomposition. You will begin with a known amount of copper metal, which, after progressing through several steps, is reproduced. In this experiment you will observe and record the various changes such as heat, color changes, and production that occur. This procedure is used to observe some chemical reactions of copper and its compounds while also performing the lab appropriately as to retain the copper as much as

The purpose of this lab was to determine the limiting reactant in a reaction between copper sulfate and iron. Using the reaction between copper sulfate and iron, the reaction was observed to see the reaction and transformation of matter. The copper sulfate was placed into a beaker, as the excess reactant, then iron filings added until the heated solution was completely reacted. This reaction created an excess of leftover. The law of conservation of mass can be observed in this reaction, and using the data found, the percent yield calculated.

11. Cu (NO3)2, cupric nitrate is used widely in industries. It makes an impersonate ink when mixed with ammonia.

Finally, we measured the mass of the remaining copper in the test tube. This lead to the discovery that the mass of the copper in relation to our original 1.08 grams of copper oxide was 0.96 grams. From this data, we could find that the measurement of oxygen in our amount of copper oxide was 0.12 grams. With these significant weights, we were then able to convert those results to the amount of moles each element had in contribution to our total quantity of copper oxide. Specifically, we found that there was 0.015 moles of copper in our copper oxide, and 0.0075 moles of oxygen. So, that made the calculated ratio between moles of copper and moles of oxygen to be 2.0, or a 2:1 ratio of copper to oxygen. Thus, the formula of the red copper oxide can be expressed as . The lab worked the way it did primarily because of the chemical characteristics of copper oxide. Since the oxygen could separate from the copper when presented with a heat source, it allowed for the amount of each element in our quantity of copper oxide to be measured and then calculated into a ratio, which determined the formula for the

-If the copper metal is submerged in the silver nitrate solution then in reaction, a pure, solid (Ag) silver product is created with an excess of (Cu (NO3)2) copper (II) aqueous liquid because a single displacement reaction occurs where the balance equation is then

Results: No substantial qualitative data was collected, except that the original reaction mixture turned a purple color. Upon the addition of anise oil and heat, the reaction mixture turned a brown color. And with the addition of NaHSO3 the mixture turned a white color. The mass of the final product sample was measured to be 0.08g (see Calculation 1). The melting point range for this sample was 172.8-185.4ºC in Trial 1 and 171.6-185.2ºC in Trial 2 (see Table 1). The IR spectrum of anise oil can be found attached. Peaks appear to exist at 3022.86, 3002.41, 2957.58, 2933.88, 2912.63, 2834.94, and 2723.19 (cm-1). Another set of peaks appear to exist at 1608.06, 1510.55, 1464.73, 1441.16, 1306.3, 1283.06, 1247.18, 1174.78, 1036.26, 964.58, 839.29, and 787.03 (cm-1). No other significant quantitative results were collected.

Before the synthesis of the Copper Iodine Compound, the identities provided (CuNO3)2 and Nal weighed 1.65 g and 4.7 g, respectively. After being weighed, the (CuNO3)2 exhibited a blue color, while the Nal, through observation, was a white color. However, when both identities were combined, the product turned into a brown and red rocky material. Once 20 mL of deionized water was added, the product quickly turned pale pink paste. After the solution was repeatedly washed with a total of an additional 100 mL of deionized water, the product was powdery and pink with small grains, and was left to air-dry. Once the product was air dried, it was observed to be a pale pink color, while the filter paper was stiff as the product was hard and dry. Therefore, the solid was scraped off onto a recrystallizing dish. However, the mass of an empty recrystallizing dish needed to be recorded in order to compare how much of the synthesized copper iodide was obtained. Within this case, the empty recrystallizing dish used weighed 32.01 g, the product on the empty dish weighed 1.03 g, having a total weight of 33.04 g.

The Copper Cycle is a popular experiment used to determine if an element, in this instance, copper, reverts to its elemental form after a chain of reactions. This experiment is very dangerous because of the reactions between the strong acids and bases. In this experiment I performed a series of reactions starting with copper metal and nitric acid to form copper (II) nitrate. Then I reacted copper and several other solutions such as, sodium hydroxide, sulfuric acid, ammonium hydroxide, and hydrochloric acid to form precipitates. In conclusion my percent recovery

Purpose: The purpose of this experiment was to observe the many physical and chemical properties of copper as it undergoes a series of chemical reactions. Throughout this process, one would also need to acknowledge that even though the law of conservation of matter/mass suggests that one should expect to recover the same amount of copper as one started with, inevitable sources of error alter the results and produce different outcomes. The possible sources of error that led to a gain or loss in copper are demonstrated in the calculation of percent yield (percent yield= (actual yield/theoretical yield) x 100.

The lab performed required the use of quantitative and analytical analysis along with limiting reagent analysis. The reaction of Copper (II) Sulfate, CuSO4, mass of 7.0015g with 2.0095g Fe or iron powder produced a solid precipitate of copper while the solution remained the blue color. Through this the appropriate reaction had to be determined out of the two possibilities. Through the use of a vacuum filtration system the mass of Cu was found to be 2.1726g which meant that through limiting reagent analysis Fe was determined to be the limiting reagent and the chemical reaction was determined to be as following:-

The zinc powder was black in colour while copper (II) sulphate solution was blue in colour because of the presence of copper (II) ions. When the zinc powder was added to the copper (II) sulphate solution and stirred, it was hard to observe the pattern of the colour change because the polystyrene cup as covered with a lid.