Deborah Bell April 17, 2012 Chemistry 1212K Lab Synthesis Report Introduction In this Chemistry Lab the main objective is to perform accurate chemical analysis for the quantity of elements and compounds in a sample. There will be a compound made then synthesized. The methods used were acid-base titrations, redox
Procedure Part I - Qualitative Analysis of Group 2 Elements Mix 0.02M K2CrO4 with each Mg(NO3)2, Ca(NO3)2, Sr(NO3)2 and Ba(NO3)2 together. Secondly, mix 0.1M (NH4)2C2O4 instead of 0.02M K2CrO4 together with the same reactants used before. Thirdly, mix 0.1M Na2SO4 with those reactants. Then, mix 0.1M NaOH with the same reactants used before again.
In this lab there was a performance of a single replacement chemical reaction. The reactants of the reaction was solid iron metal, and copper (II) sulfate solution. This was a gravimetric lab and therefore it was crucial to begin by massing the reactants individually. The copper (II) sulfate was initially a solid. A procedure was conducted to dissolve the copper (II) solid by heating it in water to create the necessary solution. Once that was complete the following action was to react the solid iron and the copper (II) sulfate solution. The single replacement chemical reaction took place and there was a replacement of copper with iron. The products of the reaction was solid copper metal and an iron (II) sulfate solution. The solid copper was
Determination of a Rate Law Megan Gilleland 10.11.2012 Dr. Charles J. Horn Abstract: This two part experiment is designed to determine the rate law of the following reaction, 2I-(aq) + H2O2(aq) +
The preparation for the experiment started by gathering the solutions of enzyme Peroxidase, substrate hydrogen peroxide, the indicator guaiacol and distilled water. Two small spectrometer tubes and three large test tubes with numbered labels. In addition, one test tube rack, one pipet pump and a box of kimwipes were also gathered. Before the experiment, the spectrometer must be set up to use by flipping the power switch to on. Following, the machine was warmed up for 10 minutes and the filter lever was moved to the left. In addition, I set the wavelength to 500 nm with the wavelength control knob. Before the experiment, I had to create the blank solution by pipetting 0.1 ml of guaiacol, 1.0 ml of turnip extract and 8.9 ml water into tube #1. Following the creation of the blank, a control 2% solution was created.
Analysis: The average deviation describes the precision of the results. It was determined the results our group obtained for were very precise. This is because our average deviation for Keq was only 6.8 which comes out to be a 6. percent error. Due to our deviation being so low it indicates
2. Write a statement to explain the molecular composition of the unknown solution based on the results obtained during testing with the Biuret solution and each sample solution.
VO3− + 4H+ + e− →VO2+ +2H2O (1) Experimental Procedure Reduction of VO3- Seven test tubes were labeled numerically with 2 mL of VO3- and H2SO42- added to each tube. A small pea size portion of solid Na2SO3 was added to the first test tube. Then, 20 drops of distilled water were added to the second test tube. In the third test tube, 20 drops of (.2 M) NaBr were added. Then, to drops of (.2 M) NaNO2 were added into the fourth test tube. A small portion of Fe(NH4)2(SO4)2 * 6H2O was added into the fifth test tube. The sixth test tube had 20 drops of (.2 M) H2Cr2O4 added, where the seventh test tube was the control tube with no additional chemicals added. All the test tubes were left to react for 3 minutes and then heated in a heated bath for approximately 20 minutes.
Kinetic study of a Solvolysis (Sn1) Reaction Aneadra Bowles Adasia Rutledge Krystal Flakes Robert Grimes Jasmine Ross June 5, 2012 Purpose: The purpose of this experiment is to use kinetics to study a solvolyis reaction
Results In experiment A the results from the precipitation of CaC2O4 H2O from the salt mixture were obtained by weighing the items listed on Table 1 on a scale.
Aim: The aim of this experiment is to observe how by increasing the temperature of sodium thiosulfate in a solution with 2.0 molar Hydrochloric acid can affect the rate of reaction and the rate in which a precipitate is formed.
Chemical Equilibrium Lab Report Aim: The aim of the lab “Chemical Equilibrium” is to observe the effects of changes in concentrations of products and reactants on the position of the equilibrium of given chemical reactions.
Summary This experiment will measure the rate of oxidation of iodide ions by persulphate ions to derive the rate law for the reaction. Starch will be added to the reaction to facilitate the measure of time during the reaction. The reactant solutions will contain (NH4)2SO4 and KI, represented as:
4) Try and propose a mechanism for the reaction using the orders of reaction taking into account the iodine, propanone and sulphuric acid.
Plan Aim: To investigate the rate of the effect of Catalase on hydrogen peroxide. Introduction This investigation will be carried out to investigate the rate of reaction of the enzyme catalase on the substrate hydrogen peroxide.