VOLUMETRIC ANALYSIS: DETERMINING THE RELATIVE MOLECULAR MASS OF A SOLUBLE BASE.

2. Write a statement to explain the molecular composition of the unknown solution based on the results obtained during testing with the Biuret solution and each sample solution.

2. To titrate a hydrochloric acid solution of “known” concentration with standardized 0.5M sodium hydroxide.

Purpose: To become familiar with the International System of Units and common laboratory equipment and techniques. To learn how to determine volume, mass, length, and temperature of a wide variety of items. To learn how to calculate density and concentration of dilutions.

Name of group or procedure Percentage composition for Mg Percentage composition for O Relatively related to the required?

2. Use the geologic definition of a mineral to determine which of the items listed in Figure 1.1 (p.3 lab book) are minerals and which are not minerals. Put an “X” in the appropriate box.

items presently in solid form in the lab kit or purchased separately for this laboratory

Using elemental analysis to determine the percent mass composition of each element in a compound is the first step in creating an empirical formula. There are many different types of elemental analysis, but in this experiment gravitational analysis and Beer’s Law are used. Elemental analysis is first used to find the moles of each element, then converted to mass, and then the percent mass of the element in the product is found (2).

11. Write the balanced chemical reaction of zinc with HCl (same as problem 5). Is the product of

3. Find a mineral in the list with the same density and hardness as your sample.

It used mass, temperature, length, volume, density, and making a dilute solution. I learned the importance as well as the difficulty of making proper measurements in a lab setting. If one measurement is off, it will throw the entire equation off. This will give either incorrect or inaccurate results.

The weight of each 50ml beaker (used for weighing the mass of dissolved Potassium chloride after the evaporation of water) should be recorded. If the experimenter were to weigh the mass of one beaker and take it as a default mass, the latter may be a source of error.

The volume of a small test tube and a thin-stemmed pipet were determined in this section of the lab. Water was poured into a small test tube until the water reached the very top edge of the test tube. The test tube was then emptied into a plastic 25 mL graduated cylinder and volume was measured and recorded into data table 3. A think-stemmed pipet was completely filled with water. Drops were carefully counted and emptied into the empty plastic 25 mL graduated cylinder until the water level reached 1 mL. The number of drops in 1 mL was recorded into data table 3. The thin-stemmed pipet had a total volume of 4 mL and that was also recorded into data table 3.

The purpose of this lab was for the student to get involved with his or hers new lab kit as well as being able to know, identify and use each other tools provided in the kit. Another key learning aspect of this lab is to teach the student how to measure properly the many units in the SI system. I will be using laboratory dilutions, measurements, and weights to then calculate using algebraic formula.

Within an acid-base titration the titration curve resembles the strengths of the corresponding acids and bases. A strong acid will correspond with a weak conjugate base, and a weak conjugate acid will correspond with a strong base. This is based on the Bronsted-Lowry model. The weak acid will donate protons to the hydroxide ion. Weak acids will have a low Ka value, the Ka value is the tendency of the acid to dissociate:

One milliliter of 6.00-M phosphoric acid was placed into a 125-mL Erlenmeyer flask using a volumetric pipette. Using a slightly larger pipette, six milliliters of 3.00-M sodium hydroxide was transferred into a 50-mL beaker. Then a disposable pipette was used to slowly mix the sodium hydroxide into the phosphoric acid while the solution was swirled around. Then both the beaker and flask were rinsed with 2-mL of deionized water and set aside. A clean and dry evaporating dish was weighed with watch glass on a scale. Then the solution was poured into the dish and the watch glass was placed on top. The solution was then heated with a Bunsen burner to allow for the water to boil off to reveal a dry white solid. After the dish cooled to room temperature it was once again weighed and the new mass was recorded.