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X-Ray Powder Diffraction Patterns

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X-ray powder diffraction patterns of good quality were obtained for the samples using CuKα radiation of wavelength 1.5406A0 at room temperature. The obtained X-ray diffraction patterns confirmed the formation of a single phase cubic spinel structure for the ferrite samples with a crystallite size ranging from 25-34nm as reported earlier [16]. The X-ray diffraction patterns were fitted using a Rietveld refinement procedure as shown in Fig 2 [17,18]. The fitted patterns were observed for eight peaks indexed by miller indices (220), (311), (222), (400), (422), (511) and (440), evident from the normal XRD patterns as reported earlier [16]. From the Fig 2 it is observed that sharpness in the peak is increased with an observed decrease in the width of the peak, which is the indication of the increase in particle size of the ferrite with the increase in Indium content. From the Fig 2 it is evident that observed patterns were exactly coinciding with the calculated values and the difference is very negligible. In comparison with the normal XRD patterns Rietveld patterns have shown some extra peaks of (331), (531), (422), (620), (533) and (622) which correspond to the second order impurity phase. The intensities of the impurity peaks reflect that the percentage of the impurity is negligible. From the Rietveld refinement patterns of the samples it is clear that the ferrites belong to the space group Fd3m with lattice parameter values ranging from 8.3106A0 to 8.3648A0. The values are in

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