4. At this point it is necessary to simultaneously moisten the cotton plug on one end of the tube with concentrated HCI, and the plug on the other end with concentrated NH3. Draw some concentrated HCl into one dropper and some concentrated NHs into another dropper. Each team member take one dropper and hold it near the cotton plugs at the opposite ends of the tube. Simultaneously touch the droppers to the respective plugs and carefully squeeze enough liquid onto the plugs to just moisten them. No liquid should be visible in the glass tube beyond the cotton plugs. If liquid is visible, the glass tube must be cleaned and dried, and the experiment repeated.

EBK A SMALL SCALE APPROACH TO ORGANIC L
4th Edition
ISBN:9781305446021
Author:Lampman
Publisher:Lampman
Chapter21: Synthesis Of N-butyl Bromide And T-pentyl Chloride
Section: Chapter Questions
Problem 1aQ
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8. Suppose in Step 4 of the Graham's law experiment one of the partners moistened the cotton on the NH3 end of the tube several seconds before the cotton on the other end was moistened. How would this mistake influence the calculated experimental value of the ratio (rate NH3)/(rate HCl)?
a. Increase it
b. Decrease it
c. Would have no effect
Explain your answer:

4. At this point it is necessary to simultaneously moisten the cotton plug
on one end of the tube with concentrated HCI, and the plug on the
other end with concentrated NH3. Draw some concentrated HCl into
one dropper and some concentrated NHs into another dropper. Each
team member take one dropper and hold it near the cotton plugs at the
opposite ends of the tube. Simultaneously touch the droppers to the
respective plugs and carefully squeeze enough liquid onto the plugs to
just moisten them. No liquid should be visible in the glass tube beyond
the cotton plugs. If liquid is visible, the glass tube must be cleaned and
dried, and the experiment repeated.
Transcribed Image Text:4. At this point it is necessary to simultaneously moisten the cotton plug on one end of the tube with concentrated HCI, and the plug on the other end with concentrated NH3. Draw some concentrated HCl into one dropper and some concentrated NHs into another dropper. Each team member take one dropper and hold it near the cotton plugs at the opposite ends of the tube. Simultaneously touch the droppers to the respective plugs and carefully squeeze enough liquid onto the plugs to just moisten them. No liquid should be visible in the glass tube beyond the cotton plugs. If liquid is visible, the glass tube must be cleaned and dried, and the experiment repeated.
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