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- Method of separation/chemical reaction (with the brief process) of 3 KG's OF SODIUM BORATE AND 1.5 KG's HYDROCHLORIC ACIDThe fat in a 1.821 g sample of potato chips is extracted with supercritical CO2. After extraction, the residue weighs 1.139 g. What is the fat content (% w/w) of the potato chips?A sample of an iron ore was prepared for Fe3+ analysis as following: 3.4g of the sample was added anddissolved in acid environment then diluted to 250 mL using volumetric flask. After that, 10 mL of the resultingsolution was transferred by pipet to a 50-mL volumetric flask and continue to be diluted. The scientists foundout that this solution gives the concentration of Fe3+ as 2.3 mg/L. Find the weight percentage of Fe3+ in theoriginal sample.
- During what century was the balance intruduced for chemicak processes?The chief chemist of the Brite-Metal Electroplating Co. isrequired to certify that the rinse solutions that are discharged from the company’s tin-plating process into the municipal sewer system contain no more than 10 ppm (parts per million) by mass of Sn2+. The chemist devises the following analytical procedure to determine the concentration. At regular intervals, a 100-mL (100-g) sample is withdrawn from the waste stream and acidified to pH = 1.0. A starch solution and 10 mL of 0.10 M potassium iodide are added, and a 25.0-mA current is passed through the solution between platinum electrodes. Iodine appears as a product of electrolysis at the anode when the oxidation of Sn2+ to Sn4+ is practically complete and signals its presence with the deep blue color of a complex formed with starch. What is the maximum duration of electrolysis to the appearance of the blue color that ensures that the concentration of Sn2+does not exceed 10 ppm?Determine the percentage Fe in a sample of limonite from the following data:Sample : 0.5000g ; KMnO4 used = 50.00 ml ; 1.000ml of KMnO4 is equivalent 0.005317 g Fe,FeSO4 used = 6.00 ml; 1.000ml FeSO4 is equivalent 0.009200 g FeO ( ans 44.59 %)
- A sample known to consist of NaOH orNaHCO3, or Na2CO3 or possible compatible mixtures of these, together with inert matter. With methyl orange, a 1.10 g sample requires 31.40 mL of HCl (of which 1.00 mL ≈ 0.0140 g CaO). With phenolphthalein, the same weight of sample requires 13.30 mL of the acid. Calculate the percentage of inert matter in the sample.What is meant by non-stoichiometric defect? Ionic solids which have anionicvacancies due to metal excess defect develop colour. Explain with the helpof suitable example.A chemist received different mixtures for analysis with the statement that they contained NaOH, NaHCO3, Na2CO3, or compatible mixtures of these substances, together with inert material. From the data given, identify the respective materials, and calculate the percentage of each component. 1.000g samples and 0.2500N HCl were used in all cases. (A) For Sample W: With PP, 24.32ml was used. A duplicate sample required 48.64ml with MO. (B). For Sample X: The addition of PP caused no color change. With MO, 38.47ml of the acid was required. (C). For Sample Y: To cause a color change in the cold with PP, 15.29ml of the acid was necessary, and an additional 33.19ml was required for complete neutralization. (D) For Sample Z: The sample was titrated with acid until the pink of PP disappeared; this process required 39.96ml. On adding an excess of the acid, boiling, and titrating back with alkali, it was found that the alkali was exactly equivalent to the excess acid added.
- A sample of iron ore weighing 800 mg was treated with HNO3 , boiled to dryness and redissolved in dilute HCl. After filtration and removal of undissolved silica, the liquid was passed through a Walden reductor. The collected sample was titrated with 0.0210 M KMnO4 , requiring 12.0 mL to reach the end point. Calc %Fe (55.845) in the ore.An acid solution containing 2 per cent by mass of NaNO3, and an unknown concentration of HNO3 is used to regenerate a strong acid resin. After sufficient acid had been passed over the resin for equilibrium to attained, analysis showed that 10 per cent of resin sites were occupied by sodium ions. What was the concentration of HNO3 in the solution, if its density were 1,030 kg/cu.m.?Pyrolusite (MnO2) is dissolved in hydrochloric acid:MnO2 + HCl → MnCl2 + H2O + Cl2The chloride was passed into potassium iodide solution where it liberated iodine:Cl2 + KI → KCl + I2The iodine liberated was estimated by adding sodium thiosulfate, the reaction beingI2 + Na2S2O3 → NaI + Na2S4O6If 5.6 g of crystallized sodium thiosulfate, Na2S2O3 5H2O ,were used up, how many grams of manganese were present?MW (g/mole): I =126.9; Mn =54.94; Cl = 35.45; K = 39.09; Na = 23; S = 32
