Which of the following would LOWER the purity of the distillate collected from the rubbing alcohol mixture? Using cold water in the condenser II. Not discarding the first milliliter distilled III. Addition of boiling chips into the mixture IV. Maintaining the temperature of the hot plate above 100°C Select one: I and II III and IV II and IV II only

Which of the following would LOWER the purity of the distillate collected from the rubbing alcohol mixture? Using cold water in the condenser II. Not discarding the first milliliter distilled III. Addition of boiling chips into the mixture IV. Maintaining the temperature of the hot plate above 100°C Select one: I and II III and IV II and IV II only

Macroscale and Microscale Organic Experiments

7th Edition

ISBN:9781305577190

Author:Kenneth L. Williamson, Katherine M. Masters

Publisher:Kenneth L. Williamson, Katherine M. Masters

Chapter7: Extraction

Section: Chapter Questions

Problem 1Q

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. Which of the following would LOWER the purity of the distillate collected from the rubbing alcohol mixture? SELECT ONE OR MORE: EXPLAIN WHY IT IS INCLUDED I. Using cold water in the condenserII. Not discarding the first milliliter distilledIII. Addition of boiling chips into the mixtureIV. Maintaining the temperature of the hot plate above 100°C
Which of the following could DECREASE the amount of the recovered crystals in the purification by recrystallization experiment? Collecting the recrystallized benzoic acid by filtration using a pre-weighed filter paper. Using a long-stemmed funnel in the hot filtration step. Cooling the filtered solution rapidly. Washing the recovered crystals using hot solvent. a. II, III b. II, IV c. II, III, IV d. I, II, III, IV
The separation and purification processes given below and the method used against them are given. Which or which of these pairings are correct? I. Brewing of tea - ExtractionII. Purification of water impurities - ChromatographyIII. Separating olive pomace from olive oil while producing olive oil-DecantationIV.Petroleum fractions obtaining - Ordinary distillationV. Obtaining essential oils and using them in perfume making - Water-steam distillationA. I, II, III, IVB. I, II, III, IV, VC. I, IV, VD. I, II, III, VE. I, II, V
6.0 mL of cyclohexanol, 8 mL of 85% phosphoric acid, and 10 drops of sulfuric acid are added to a 50-mL round-bottom flask with boiling chips, and the mixture is distilled into an ice-cooled receiver. The distillate is in the form of a colorless bi-phasic mixture. The cyclohexene upper layer is removed from the water layer, and dried over anhydrous calcium chloride. Isolated is cyclohexene as a clear and colorless foul-smelling liquid. Weighing data is given below. Gross mass: 51.24 g Tare mass: 48.04 g Product mass: 3.2g Question: Calculate the theoretical mass of the cyclohexene product, bearing in mind that the cyclohexanol starting material was measured by volume, not by mass (so you must use the density of cyclohexanol to convert milliliters to grams, before calculating the number of moles). Calculate the percent yield of cyclohexene obtained.
You were given a mixture of two miscible solvent A and B that you are tasked to separate. You know that solvent A has a boiling point of 49 oC while solvent B has a boiling point of 174 oC. Which of the listed method would overall be the most efficient? Fractional distillation Recrystallization Solid-liquid extraction Liquid-liquid extraction Simple distillation Acid-Base extraction
A mixture of 5 mL of acetone (boiling point 56 ° C) and toluene (boiling point 111 ° C) was separated by fractional distillation. At the end of the distillation, 2.5 mL of the fraction 1 and 1.6 mL of fraction 2. The percent recovery of toluene is: a.39% b.50% C.32% d.82%
1. Which of the following may cause an increase in the calculated percent recovery of the recrystallized benzoic acid? a.Adding too much solvent in the receiving flask during hot filtrationb.Using cold water in rinsing the residue from the flask during hot filtration c.Using fluted filter paper during hot filtrationd.Not adding animal charcoal to the solution2. Which set of reagents can confirm that sulfate ions are present in two unkown solutions? a.1.0 M NaOH and excess NH3 b.0.1 M Ba(NO3)2 and 0.01 M KMnO4 c.1.0 M NaOH and 0.1 M K2Zn3[Fe(CN)6]2d.0.1 M Ba(NO3)2 and 1.0 M CH3COOH
A 0.100 gram sample of phthalic acid was dissolved in 100 mL of water. When 25 of diethyl ether was used to extract the phthalic acid, 0.042 grams of phthalic acid re recovered. What is the distribution coefficient for this extraction Kp?
Neel’s unknown solid 1) dissolves in hot ethanol, 2) is essentially insoluble in hexane, and 3) is insoluble in cold water, but sparingly soluble in warm water. Outline a recrystallization procedure.
Acetophenone is soluble in diethyl ether, isopropanol, and n-hexane. Identify and justify the most suitable solvent for UV-Vis characterization
Acetophenone is soluble in diethyl ether, isopropanol, and nhexane. Identify and justify the most suitable solvent for UV- Vis characterization?
MAKE A METHODOLOGY : MATERIALS/ REAGENTS WITH SCHEMATIC DIAGRAM . THE PICTURE UPLOADED SERVES AS A GUIDE, DO THE SAME THING BASED FROM THE PIC. Procedure: Place 20 drops of each of 0.2M CuSO4 in a centrifuge tube. Then add 5 drops of freshly prepared 6M (NH4)2S to each centrifuge tube. Record your observation. Centrifuge the mixtures for 3 mins. and decant the supernatant liquid. Add 10 drops of DI water and 10 drops of 6M HNO3. Stir and boil the mixture in a hot water bath for 5 mins. centrifuge the mixture for 3 mins. Decant the supernatant solution from procedure 3. Discard the To each of the supernatant liquid, add 6 drops of 6M H2SO4. Allow themixtures to cool and 5 drops of DI water. To the mixtures in procedure 4, add few drops of concentrated NH3 until the solution becomes basic. Confirm using a litmus paper. Record your observation. Add 1 drop of 5M NaOH and 1 drop of 0.1 M SnCl2 to the centrifuge tube containing Bi3+ ion , centrifuge and decant the supernatant liquid. To…