Racemic Mixtures Lab Report

Title: Separation Lab Purpose: The purpose of this lab was to successfully separate a mixture of iron filings, poppy seeds, sand and salt. Hypothesis: In my opinion, I think it is possible to successfully separate the mixture.

This could be improved by utilizing an inert atmosphere of solely nitrogen. Melting the compound resulted in an intensely dark purple liquid. This is a result of the resonance stabilized radical being formed by the homolysis of the carbon-to-carbon bond validating the photochromic properties. The colour change further substantiates that the desired product was produced despite the inaccuracies in melting point values. Homolytic cleavage of the dimer prepared by solvation with toluene results in a deep purple solution confirming the formation of the resonance stabilized radical.

Experiment 55 consists of devising a separation and purification scheme for a three component mixture. The overall objective is to isolate in pure form two of the three compounds. This was done using extraction, solubility, crystallization and vacuum filtration. The experiment was carried out two times, both of which were successful.

Aim: The aim of the lab “Chemical Equilibrium” is to observe the effects of changes in concentrations of products and reactants on the position of the equilibrium of given chemical reactions.

There are millions of different organic compounds. Most of them are found in mixtures and in order to achieve a pure form they need to be separated, isolated, and purified. However, there are endless numbers of possible mixtures, which make it impossible to have a pre-designed procedure for every mixture. So chemists often have to make their own procedures. The purpose of this experiment was to prepare the student to the real world by them designing their own procedure which will help them understand the techniques of separation and purification better. The goal was to extract two of the components of the

Abstract: One mixture of two unknown liquid compounds and one mixture of two unknown solid compounds were separated, isolated, purified, and characterized by boiling point. Two liquid unknowns were separated, isolated, and purified via simple distillation. Then, the process of an acid-base extraction and washing were used to separate two unknown compounds into two crude compounds: an organic acid and a neutral organic compound. Each crude compound was purified by recrystallization, resulting in a carboxylic acid (RCO2H) and a pure organic compound (RZ). The resulting mass of the pure carboxylic acid was 1.688g with a percent recovery of 31.80%, the boiling range was 244-245 °C, and its density was 2.0879g/mL. The resulting mass of the pure organic solid was 2.4902g with a percent recovery of 46.91%, the boiling range was 52.0-53.4°C, and its density was 1.5956 g/mL.

After completing the experiment, a yield of 0.01 g of an impure, solid purple, precipitate was created, however this yield will not be considered for percent yield or for future use due to its impurity in nature. This conclusion on the purity of the substance is drawn from the information for pure tetraphenylcyclopentadienone; pure tetraphenylcyclopentadienone has a characteristic black/purple tint to its crystals, and said crystals are very small, almost sand-like in state1. Comparing this description to the description of the experimental sample, a clear main difference is the tint of the color, which was solid purple as opposed to the expected black/purple (this purple tint may

Someone hands you a container of a mysterious white mixture, and they give you the task to figure out what it is. What would you do to solve the problem at hand? Many scientists might find physical and chemical properties to figure it out. The scientists might look for, odor change, temperature change, fizzing, and bubbling for chemical properties. They also inspect the mixtures for physical properties before a chemical reaction occurs, including shape, size, color, texture, and smell. The Eighth grade thinks that the mystery mixture is C6H8O7(Citric Acid) and NaHCO3(Baking Soda).

From the results that were acquired from mixing the liquid reagents with each powder, it was determined that Unknown Mixture #1 consisted of baking soda and cornstarch. When individually testing the substances from Unknown Mixture #1 with the liquid reagents, a few noticeable reactions occurred. Mixing baking soda with vinegar caused bubbling to occur. This is because a neutralization reaction took place between the two reactants. In this reaction, sodium bicarbonate(baking soda) reacts with vinegar and produces sodium acetate, water, and carbon dioxide(HC2H3O2(aq) + NaHCO3(aq) NaC2H3O2(aq) + H2O(l) + CO2(g) ). The gaseous carbon dioxide most likely tried to escape into the atmosphere and caused the bubbling to occur. Another noticeable reaction

Background: Mixtures are combinations pure substances, thus their physical properties depend on their composition. Physical properties of a pure substance include solubility, conductivity, and magnetism. By exploiting unique properties of mixtures, it is possible to divide the mixture into its components. This is done by physical change, such as filtration, evaporation, and crystallization.

Identifying the three components of the unknown mixture, a 1.5 g sample was obtained and dissolved in 30 mL of diethyl ether. This solution was then poured into a separatory funnel with a funnel with the stopcock closed, and inverted twice so that there would be a formation of different layers in the mixture. In order to extract the base from the mixture, approximately 14 mL of 10% hydrochloric acid was added into the funnel and mixed. To mix the hydrochloric acid thoroughly the funnel was gently shaken with the pressure released by removing the stopper intermittently. The solution then separated into an aqueous layer at the bottom, and an organic layer at the top (containing the acid).1 The aqueous layer (containing the base) was released into an

The cup got colder, was a endothermic reaction, which used up energy from the environment, sucked the heat out.

The aim of this experiment is to use separation techniques to separate a mixture containing polystyrene beads, salt, sand, gravel and iron filings.

The purpose of this experiment is to separate a mixture of salicylic acid and naphthalene using extraction, recrystallization and sublimation techniques. Extraction is the separation of compounds from a mixture based on their relative solubilities in different solvents. Sublimation is the process of separation by which a substance transitions from the solid phase into the gas phase, skipping the liquid phase. Recrystallization involves dissolving a substance in an appropriate solvent then crystallizing it as it cools (impurities remain in solution). The melting points of the substances were determined in order to assess their purity and the percent recovery of pure naphthalene and salicylic acid were calculated. According to the results, the melting point of pure naphthalene was between 86°C -89°C range, whereas for pure salicylic acid was 167°C -170°C. Both determined melting points were higher compared to the literature value of 80.26°C and 158.6°C for pure naphthalene and salicylic acid respectively. Lastly, the percent recovery for pure naphthalene and salicylic acid were 17.7% and 71.2% accordingly.

Subsequently, 10mL of 3.5% H2O2 were added dropwise to the reaction mixture and was stirred for 20 minutes before heating to boiling at 80°C for 5 minutes. The reaction mixture was then taken off heat and allowed to cool undisturbed in an ice-bath for 30 minutes. Suction filtration was performed after to collect the crystals from the chilled solution The product was then washed with chilled 95% ethanol (2 x 15mL) and followed by diethyl ether (2 x 10mL). The crude product was then left to dry before recording the yield. 20mg of the crude product is then accurately weighed out and dissolved in deionized water in a 25mL volumetric flask. Deionized water was added to the volumetric flask to the mark and the UV-vis absorption spectrum of the crude product was recorded.