1. NH3, pyridine `NH2 2. LIAIH4, Et2O 3. H* workup 1. SOCI2 2. ELOH OEt 1. CrO3, pyridine NH2 2. pH 5

Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter29: Supercritical Fluid Chromatography And Extraction
Section: Chapter Questions
Problem 29.11QAP
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1. NH3, pyridine
NH2
2. LIAIH4, Et20
3. H* workup
1. SOCI,
2. ELOH
OEt
1. CrO3, pyridine
NH2
2.
, рH 5
1.CrОз, Н2О
OMe
2. МеОН, Н* cat.
1. PhMgBr (excess), Et,0
2. H* workup
Ph
Ph
3.
H* cat.
Transcribed Image Text:1. NH3, pyridine NH2 2. LIAIH4, Et20 3. H* workup 1. SOCI, 2. ELOH OEt 1. CrO3, pyridine NH2 2. , рH 5 1.CrОз, Н2О OMe 2. МеОН, Н* cat. 1. PhMgBr (excess), Et,0 2. H* workup Ph Ph 3. H* cat.
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