1.1.5. RESULTS & ANALYSIS 1. Fill out the information in the table below. Substance 1. Pure Urea 2. Pure Cinnamic Acid 3.75 Urea-25C.A% 4.50Urea-50C.A% 5.25Urea-75C.A% Initial Melting Temp. °C 133 134 94 95 98 Set Point 120° (1,2) set Point = 90° (3,4,5) Melting Range Final Melting Temp. °C 136 137 130 100 109 = 3 3 36 5 11 On a separate graph paper sketch a graph of the eutectic point diagram using the mole fractions calculated above as the X-axis and the melting point Temperatures as Y-axis.
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- 50 mg of granular salt is briefly stirred into a glass container of 1/5 liter volume filled with water. After briefly mixing, some salt is still seen at the bottom of the class. The visible salt is filtered from the water, weighed and determined to have a mass of 20 mg. What is the dissolved phase concentration of salt remaining in the water? Provide your answer to the nearest whole number in units of mg/l.Q3 / The solubility of sodium chloride NaCl in water at 290 Kis 35.8 kg / 100 kg of water. Express the solubility as the following: 1. Mass fraction and the mass percent of Naci 2. Mole fraction and mole percent of NaCl 3. kmol of NaCl per 1000 kg of water Note: molecular weight of NaCl = 135.8, and water = 18.016A solution of common salt in water is prepared by adding 50kg of salt to 200kg of water tomake a liquid density of 1250kg/m3. Calculate the concentration of salt in this solution as a: i) Weight(w/w)fraction (Ans: weight fraction 20%)
- 125.1 mg of streptomycin sulphate are dissolved in 10 ml of water. A GC headspace analysis is carried out in order to determine the methanol content of the drug. A peak for methanol is produced which has 73.2% of the area of a peak for a methanol standard containing 0.532 mg/100 ml of methanol in water analysed under exactly the same conditions, What is the methanol content of the streptomycin sulphate in ppm and %w/w? Answer: 311.3 ppm, 0.3113 % w/w.how??Bristol Community College Fall River, Massachusetts Experiment 6: Molar Mass of a Molecular Solid from Freezing Point-Depression Measurement Name: __________________________________ Date: _______________ Approved: ___________ DATA SHEET Mass of lauric acid (in Part II) Mass of benzoic acid (in Part II) Freezing temperature of pure lauric acid (from Part I) data from Video 2 of Part I Freezing temperature of solution (from Part II) data from Video referenced in Part II Freezing point depression, Tf ( = Tf, lauric acid – Tf, solution) Molality (m) of solution ( Eq. 1) Moles of benzoic acid ( Eq. 2) Experimental molar mass of benzoic acid (Eq. 3) Calculate the molar mass of benzoic acid, C6H5COOH. Percent error Summary Questions A student determines…Gypsum (CaSO4) is one of common precipitants in brackish water desalination processes. CaSO4 ⇋ Ca2+ + SO42- Ksp = 10-4.6Assume a water containing: [Ca2+] = 10-2.1 M; [SO42-] = 10-3.2 M.(a) Find Qsp or IAP for the given water. (b) Find the solubility index (SI) and determine whether CaSO4 is under, super, or at saturation in the water.
- If we draw operation line diagram, Compositions of 2 phases are represented in a 2-D graph. Does operation line always be a line?Boiling Point Elevation/Freezing Point Depression T = m K where, for freezing point depression: T = T(pure solvent) - T(solution) and for boiling point elevation: T = T(solution) - T(pure solvent) m = (# moles solute / Kg solvent) Kb = boiling point elevation constant. Kf = freezing point depression constant. Kb and Kf depend only on the SOLVENT. Below are some common values. Use these values for the calculations that follow. Solvent Formula Kb(°C / m) Kf(°C / m) Water H2O 0.512 1.86 Ethanol CH3CH2OH 1.22 1.99 Chloroform CHCl3 3.67 Benzene C6H6 2.53 5.12 Diethyl ether CH3CH2OCH2CH3 2.02(This question and the next 2 questions are breakdowns of the same question) A student John wanted to measure the molar mass of an unknown material (UM) via the boiling point change of a solvent. He chose a solvent, ethanol, that can dissolve the material and sugar. He wanted to use sugar (MW = 342.3 g/mol) as a reference sample to get an ebullioscopic constant for his system to reduce the effect of other measuring errors such as pressure, measuring errors, and impurity of the samples. He made 10 solutions each contain 100 g of ethanol and various amont of solute as list in the table. He fits the two sets of data and obtain the molar weight of the unknown materials. For this question answer the fitted boiling point of pure ethanol: ____ K. 4 sig. fig. Thre rest ? marks in the tale will be answered in the next two questions. Copy the data into Excel and use trendline to fit or calculate the average values for this and the next 2 questions. Sample # Sugar (g) B.P. (K) Sample # UM…
- 200 mg of granular salt is briefly stirred into a glass container of 1/2 liter volume filled with water. After briefly mixing, some salt is still seen at the bottom of the class. The visible salt at the bottom of the glass is filtered from the water, weighed and determined to have a mass of 50 mg. What is the dissolved phase concentration of salt remaining in the water? Provide your answer to the nearest whole number in units of mg/l.Referring to the Al-Si Eutectic diagram discussed on the Phase Diagrams-Lever Rule handout, calculate the mass fraction of the phase, silicon, given a sample with 51.7 wt% aluminum at 576.99 ˚C.3. Refer to the phase diagram depicted below: When 7 moles of A and 3 moles of B are mixed at 50oC which is then cooled to 10oC the sample turns into two liquid phases, phase I has mole fraction xB=0.14 (see diagram below). Find the phase II mole fraction xB, and then calculate the ratio of amount of substance in phase I to that in phase II using Lever rule. Please enter your answer as a number with two decimals. for example, if the ratio you calculated is 2:3, you enter as 0.67