2. 3. 4. Ph. OTBS + Ph + of CN 1. Ac₂0 2. NaOH CN 1. n-BuLi && 2. PPh3 OTf Me NaH Me PÅH Ph dioxane, reflux PhSH H OTBS Me Me NH₂

Fundamentals Of Analytical Chemistry
9th Edition
ISBN:9781285640686
Author:Skoog
Publisher:Skoog
Chapter16: Applications Of Neutralization Titrations
Section: Chapter Questions
Problem 16.34QAP
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2.
3.
4.
Ph.
OTBS
&
PPh3
+
S.
+ Ph
OTf
-CN
CN
1. Ac₂0
2. NaOH
1. n-BuLi
2.
Me.
NaH
Me
dioxane, reflux
Ph
H
H
PhSH
OTBS
Me
Me
NH₂
Transcribed Image Text:2. 3. 4. Ph. OTBS & PPh3 + S. + Ph OTf -CN CN 1. Ac₂0 2. NaOH 1. n-BuLi 2. Me. NaH Me dioxane, reflux Ph H H PhSH OTBS Me Me NH₂
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