2A. What is the theoretical yield and limiting reagent for the Friedel Crafts acylation reaction of toluene as described in the experiment provided if the reaction is started with 5 g of aluminum chloride, 25 mL of dichloromethane (total), 3.5 g acetyl chloride, and 3.7 mL of toluene? 2B. What are the safety precautions used in the experimental procedure provided to prevent exposure to HCI gas? 2C. Write the separation scheme for the isolation of 4-methyl acetophenone from the reaction mixture in the experiment provided.

Macroscale and Microscale Organic Experiments
7th Edition
ISBN:9781305577190
Author:Kenneth L. Williamson, Katherine M. Masters
Publisher:Kenneth L. Williamson, Katherine M. Masters
Chapter43: Amines
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Please answer 2C (see 2a and 2b for information supporting it)

2A. What is the theoretical yield and limiting reagent for the Friedel Crafts acylation reaction of toluene
as described in the experiment provided if the reaction is started with 5 g of aluminum chloride, 25 mL
of dichloromethane (total), 3.5 g acetyl chloride, and 3.7 mL of toluene?
2B. What are the safety precautions used in the experimental procedure provided to prevent exposure
to HCI gas?
2C. Write the separation scheme for the isolation of 4-methyl acetophenone from the reaction mixture
in the experiment provided.
Transcribed Image Text:2A. What is the theoretical yield and limiting reagent for the Friedel Crafts acylation reaction of toluene as described in the experiment provided if the reaction is started with 5 g of aluminum chloride, 25 mL of dichloromethane (total), 3.5 g acetyl chloride, and 3.7 mL of toluene? 2B. What are the safety precautions used in the experimental procedure provided to prevent exposure to HCI gas? 2C. Write the separation scheme for the isolation of 4-methyl acetophenone from the reaction mixture in the experiment provided.
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