An ore containing magnetite, Fe3O4 was analyzed by dissolving a 1.5419 g sample in concentrated HCl, giving a mixture of Fe2+ and Fe3+. After adding HNO3 to oxidize any Fe2+ to Fe3+, the resulting solution was diluted with water and the Fe3+ precipitated as Fe(OH)3 by adding NH3. After filtering and rinsing, the residue was ignited, giving 0.8525 g of pure Fe2O3. Calculate the %w/w Fe3O4 in the sample.
An ore containing magnetite, Fe3O4 was analyzed by dissolving a 1.5419 g sample in concentrated HCl, giving a mixture of Fe2+ and Fe3+. After adding HNO3 to oxidize any Fe2+ to Fe3+, the resulting solution was diluted with water and the Fe3+ precipitated as Fe(OH)3 by adding NH3. After filtering and rinsing, the residue was ignited, giving 0.8525 g of pure Fe2O3. Calculate the %w/w Fe3O4 in the sample.
Chemistry: Principles and Practice
3rd Edition
ISBN:9780534420123
Author:Daniel L. Reger, Scott R. Goode, David W. Ball, Edward Mercer
Publisher:Daniel L. Reger, Scott R. Goode, David W. Ball, Edward Mercer
Chapter19: Transitition Metals, Coordination Chemistry And Metallurgy
Section: Chapter Questions
Problem 19.65QE
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An ore containing magnetite, Fe3O4 was analyzed by dissolving a 1.5419 g sample in concentrated HCl, giving a mixture of Fe2+ and Fe3+. After adding HNO3 to oxidize any Fe2+ to Fe3+, the resulting solution was diluted with water and the Fe3+ precipitated as Fe(OH)3 by adding NH3. After filtering and rinsing, the residue was ignited, giving 0.8525 g of pure Fe2O3. Calculate the %w/w Fe3O4 in the sample.
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