Based on your observations in Part III, which reagent is present in excess? Which reagent is the Limiting Reagent (completely used up)? Calculate the theoretical yield of [Ni(en)3]Cl₂ upon your assumption of the Limiting Reagent. Calculate the theoretical yield of [Ni(en)3] Cl₂ using the excess reagent. Did your observations with your agree calculations? Calculate the percent yield of the [Ni(en)3] Cl₂.

Fundamentals Of Analytical Chemistry
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Chapter26: Molecular Absorption Spectrometry
Section: Chapter Questions
Problem 26.14QAP
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DATA ANALYSIS & DISCUSSION
CALCULATIONS & DETERMINATIONS
Based on your observations in Part III, which reagent is present in excess? Which reagent is the
Limiting Reagent (completely used up)?
Calculate the theoretical yield of [Ni(en)3] Cl₂ upon your assumption of the Limiting Reagent.
Calculate the theoretical yield of [Ni(en)3] Cl₂ using the excess reagent.
Did your
observations agree with your calculations?
Calculate the percent yield of the [Ni(en)3] Cl₂.
DISCUSSION
1. Summarize the results of this experiment.
2. What is the quality of the results? Do the results seem reasonable?
3. What were the errors or possible errors in the experiment?
4. How would the errors affect the results of the experiment?
Transcribed Image Text:DATA ANALYSIS & DISCUSSION CALCULATIONS & DETERMINATIONS Based on your observations in Part III, which reagent is present in excess? Which reagent is the Limiting Reagent (completely used up)? Calculate the theoretical yield of [Ni(en)3] Cl₂ upon your assumption of the Limiting Reagent. Calculate the theoretical yield of [Ni(en)3] Cl₂ using the excess reagent. Did your observations agree with your calculations? Calculate the percent yield of the [Ni(en)3] Cl₂. DISCUSSION 1. Summarize the results of this experiment. 2. What is the quality of the results? Do the results seem reasonable? 3. What were the errors or possible errors in the experiment? 4. How would the errors affect the results of the experiment?
NTH
assign one of the Trials to pe
iment. Upon completion of your exper
Volume (mL)
7.0
NICI₂6 H₂O
mass of Nicl₂ •64₂0= 2.80
volume of 4.0 M C₂ 48 W₂ = 7.5
1
7.5
mass of witch glass 29.7189
mass of prodiect & watch ghasi
31.9739
mass of the product: 2.269.
the pH is a light green
& a 7 on the scale.
Tria (3)
shade.
0
the beaker until you obtai
ation of the solid.
filtrate in filter blask is pick-
Lavener so C₂ 48 No is the excers
reasent
opwise to the solid unti
mL. Record your obses
10 mL graduated cyli
7. Pour
tion beaker,
dropwise to the bea
all of the solution,
ges observed dur
Ni Cl₂ · 6 Fl₂0 was the lumiting vergent.
sti
da second 5 mL aliquot
RECOVE
AL beaker
th the ace
ted cyli
the be
5 mL aliquot of acetone to the
Transcribed Image Text:NTH assign one of the Trials to pe iment. Upon completion of your exper Volume (mL) 7.0 NICI₂6 H₂O mass of Nicl₂ •64₂0= 2.80 volume of 4.0 M C₂ 48 W₂ = 7.5 1 7.5 mass of witch glass 29.7189 mass of prodiect & watch ghasi 31.9739 mass of the product: 2.269. the pH is a light green & a 7 on the scale. Tria (3) shade. 0 the beaker until you obtai ation of the solid. filtrate in filter blask is pick- Lavener so C₂ 48 No is the excers reasent opwise to the solid unti mL. Record your obses 10 mL graduated cyli 7. Pour tion beaker, dropwise to the bea all of the solution, ges observed dur Ni Cl₂ · 6 Fl₂0 was the lumiting vergent. sti da second 5 mL aliquot RECOVE AL beaker th the ace ted cyli the be 5 mL aliquot of acetone to the
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