Data and Calculations: Determination of the Hardness of Water 112.580 Volume Ca* solution prepared Mass of beaker plus CaCO, Mass of beaker less sample Caco 0.1 A 1 g Molarity of Ca²+ Moles Ca²+ in each 250 ml. M

Fundamentals Of Analytical Chemistry
9th Edition
ISBN:9781285640686
Author:Skoog
Publisher:Skoog
Chapter31: Introduction To Analytical Separations
Section: Chapter Questions
Problem 31.32QAP
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Data Given. no Trial 3 information needed

Experiment 28
Data and Calculations: Determination of the Hardness of Water
Mass of beaker
plus CaCO,
Mass of beaker
less sample
Mass of CaCO3
sample
Number of moles CaCO3 in sample
(Formula mass = 100.1 g/mol)
Determination of blank:
Initial buret
reading
Standardization of EDTA Solution
Titration
Initial buret reading
Final buret reading
Volume of EDTA
O
Volume of EDTA used to
titrate blank
Volume of EDTA used to
titrate Ca2+
Molarity of EDTA =
moles Ca2+ in aliquot × 1000
volume of EDTA required (mL)
Mean molarity of EDTA:
112.590
0.1
0.4
Final buret
mL reading
I
10.5
35
245
g
g
moles
11
2
mL
mL
mL
mi.
mL
M
Volume Ca*
solution prepared
Molarity of Ca²+
Moles Ca²+ in each
aliquot titrated
mL
II
35
Volume
of blank
O
35
mL
mL
mL
mL
250
mL
M
51
III
M Standard deviation in molarity of EDTA:
mL
M
moles
mL
mL
mL
mL
mL
mL
M
M
(continued on following page
Transcribed Image Text:Experiment 28 Data and Calculations: Determination of the Hardness of Water Mass of beaker plus CaCO, Mass of beaker less sample Mass of CaCO3 sample Number of moles CaCO3 in sample (Formula mass = 100.1 g/mol) Determination of blank: Initial buret reading Standardization of EDTA Solution Titration Initial buret reading Final buret reading Volume of EDTA O Volume of EDTA used to titrate blank Volume of EDTA used to titrate Ca2+ Molarity of EDTA = moles Ca2+ in aliquot × 1000 volume of EDTA required (mL) Mean molarity of EDTA: 112.590 0.1 0.4 Final buret mL reading I 10.5 35 245 g g moles 11 2 mL mL mL mi. mL M Volume Ca* solution prepared Molarity of Ca²+ Moles Ca²+ in each aliquot titrated mL II 35 Volume of blank O 35 mL mL mL mL 250 mL M 51 III M Standard deviation in molarity of EDTA: mL M moles mL mL mL mL mL mL M M (continued on following page
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