// Deduce the coupling partners in the aliphatic region of Glutamic Acid from the cosy given. Assign the peaks. 19 OH =O (B) 6 2.20 2.40 2.60 2.80 3.00

Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter21: Surface Characterization By Spectroscopy And Microscopy
Section: Chapter Questions
Problem 21.10QAP
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all Deduce the
Coupling partners
in the aliphatic
region of
Acid
Glutamic
from the cosy given.
Assign the peaks.
8
503)
OH
H₂N
OH
(B)
6
2.20
2.40
2.60
2.80
3.00
3.20
3.40
3.60
3.80
4.00
4.00 3.80 3.60 3.40 3.20 3.00 2.80 2.60 2.60 2.20 6
Fig. 2. 500 MHz COSY spectrum of glutamic acid (B) in D₂O as a contour plot.
At the left-hand edge and at the top is the one-dimensional ¹H NMR Spectrum.
Transcribed Image Text:all Deduce the Coupling partners in the aliphatic region of Acid Glutamic from the cosy given. Assign the peaks. 8 503) OH H₂N OH (B) 6 2.20 2.40 2.60 2.80 3.00 3.20 3.40 3.60 3.80 4.00 4.00 3.80 3.60 3.40 3.20 3.00 2.80 2.60 2.60 2.20 6 Fig. 2. 500 MHz COSY spectrum of glutamic acid (B) in D₂O as a contour plot. At the left-hand edge and at the top is the one-dimensional ¹H NMR Spectrum.
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