For the NMR spectrum shown below", draw the structure of the reactant next to the spectrum and label the protons so that they match the letter labels shown on the NMR spectrum. Fill in the Chemical shift, integration and multiplicity in the table. You may want to complete sections c) and d) before assigning the aromatic ring protons. B Integration-2 There is a very broad (almost flat) signal here. Appears to be a singlet Integration-1 14 HSP-04-502 STRUCTURE: 12 10 ppm Integration-2 D Broad singlet Integration ~ 2 Proton Chemical shift Relative integration Multiplicity label (ppm) A B CD

EBK A SMALL SCALE APPROACH TO ORGANIC L
4th Edition
ISBN:9781305446021
Author:Lampman
Publisher:Lampman
Chapter59: Preparation Of A C-4 Or C-5 Acetate Ester
Section: Chapter Questions
Problem 6Q
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1.
This question deals with the reactant used in this experiment 4-aminobenzoic acid.
a.
For the IR spectrum shown below*, identify the structural features which cause the
indicated IR signals.
100
4000
3000
2000
300
2000
500
ARVENUMBER
Transcribed Image Text:1. This question deals with the reactant used in this experiment 4-aminobenzoic acid. a. For the IR spectrum shown below*, identify the structural features which cause the indicated IR signals. 100 4000 3000 2000 300 2000 500 ARVENUMBER
b.
For the NMR spectrum shown below*, draw the structure of the reactant next to the spectrum and label the protons so
that they match the letter labels shown on the NMR spectrum. Fill in the Chemical shift, integration and multiplicity in
the table. You may want to complete sections c) and d) before assigning the aromatic ring protons.
B
Integration-2
There is a very broad
(almost flat) signal here.
Appears to be a singlet
Integration - 1
14
12
10
HSP-04-502
STRUCTURE:
Integration-2
D
Broad singlet
Integration
2
ppm
Proton
Chemical
shift Relative integration
Multiplicity
label
(ppm)
с
D
ABCC
А
В
Transcribed Image Text:b. For the NMR spectrum shown below*, draw the structure of the reactant next to the spectrum and label the protons so that they match the letter labels shown on the NMR spectrum. Fill in the Chemical shift, integration and multiplicity in the table. You may want to complete sections c) and d) before assigning the aromatic ring protons. B Integration-2 There is a very broad (almost flat) signal here. Appears to be a singlet Integration - 1 14 12 10 HSP-04-502 STRUCTURE: Integration-2 D Broad singlet Integration 2 ppm Proton Chemical shift Relative integration Multiplicity label (ppm) с D ABCC А В
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