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How can we know that the NMR for cyclohexanone is in fact cyclohexanone( the NMR for cyclohexanone is not labeled). Analyze the spectra to prove

How can we know that the NMR for cyclohexanone is in fact cyclohexanone( the NMR for cyclohexanone is not labeled). Analyze the spectra to prove

Fundamentals Of Analytical Chemistry
Fundamentals Of Analytical Chemistry
9th Edition
ISBN:9781285640686
Author:Skoog
Publisher:Skoog
Chapter7: Statistical Data Treatment And Evaluation
Section: Chapter Questions
Problem 7.9QAP
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An oxidation reaction was conducted using cyclohexanol and NaOCl to make cyclohexanone. How can we know that the NMR for cyclohexanone is in fact cyclohexanone( the NMR for cyclohexanone is not labeled). Analyze the spectra to prove its identity along with the NMR of the starting material which is the spectra labeled cyclohexanol below.

471 BRUKER I222 |TV || Current Data Paramet ers Feb20-2020-chem22: 67 NAME EXPNO PROCNO 1 Cyclohexanol in CDC13 F2 - Acquisition Parameter Date Time 20200220 23.13 INSTRUM PROBHD spect 5 mm PABBO вв- zg30 32768 PULPROG TD SOLVENT NS CDC13 2 DS SWH 5208.333 Hz 0.158946 Hz 3.1457281 sec 16 96.000 usec 25.61 usec 298.0 K FIDRES AQ RG DW DE ТЕ D1 1.50000000 sec TDO 1 ------- CHANNEL f1 NUC1 P1 -- - - 1H 11.38 usec -2.50 dB 18.35869598 w PL1 PL1W SFO1 400.1320007 MH2 F2 - Processing parameters SI SF 32768 400.1300065 MHz WDW SSB EM 0.30 Hz LB GB PC 1.00 7.5 7.0 6.5 6.0 5.5 5.0 4.5 4.0 3.5 3.0 2.5 2.0 1.5 1.0 ppm 888
Transcribed Image Text:471 BRUKER I222 |TV || Current Data Paramet ers Feb20-2020-chem22: 67 NAME EXPNO PROCNO 1 Cyclohexanol in CDC13 F2 - Acquisition Parameter Date Time 20200220 23.13 INSTRUM PROBHD spect 5 mm PABBO вв- zg30 32768 PULPROG TD SOLVENT NS CDC13 2 DS SWH 5208.333 Hz 0.158946 Hz 3.1457281 sec 16 96.000 usec 25.61 usec 298.0 K FIDRES AQ RG DW DE ТЕ D1 1.50000000 sec TDO 1 ------- CHANNEL f1 NUC1 P1 -- - - 1H 11.38 usec -2.50 dB 18.35869598 w PL1 PL1W SFO1 400.1320007 MH2 F2 - Processing parameters SI SF 32768 400.1300065 MHz WDW SSB EM 0.30 Hz LB GB PC 1.00 7.5 7.0 6.5 6.0 5.5 5.0 4.5 4.0 3.5 3.0 2.5 2.0 1.5 1.0 ppm 888
3 ... BRUKER Current Data Paramet ers NAME EXPNO Feb18-2020-chem22: 3 PROCNO 1 F2 - Acquisition Paramet er Date_ Time INSTRUM PROBHD 20200218 17.31 spect 5 mm PABBO BB- zg30 32768 CDC13 2 1.8 1.7 1.6 ppm PULPROG TD SOLVENT 2.9 2.8 2.7 2.6 2.5 2.4 2.3 2.2 2.1 2.0 1.9 NS DS SWH 5208.333 Hz 0.158946 Hz 3.1457281 sec 64 96.000 usec FIDRES AQ RG DW DE 25.61 usec 298.0 K 1.50000000 sec 1 TE D1 TDO CHANNEL f1 =-- 1H 11.38 usec -2.50 dB 18.35869598 W 400.1320007 MH2 ===== =- NUC1 P1 PL1 PL1W SFO1 F2 - Processing parameterS 32768 400.1300065 MHz SI SF WDW EM SB LB 0.30 Hz GB PC 1.00 11 10 8 7 6 5 4 3 2 1 ppm 000' 2.32 1.044 -2.08 88:I 98:T/ 1.85 1.70 1.70 69'I 89
Transcribed Image Text:3 ... BRUKER Current Data Paramet ers NAME EXPNO Feb18-2020-chem22: 3 PROCNO 1 F2 - Acquisition Paramet er Date_ Time INSTRUM PROBHD 20200218 17.31 spect 5 mm PABBO BB- zg30 32768 CDC13 2 1.8 1.7 1.6 ppm PULPROG TD SOLVENT 2.9 2.8 2.7 2.6 2.5 2.4 2.3 2.2 2.1 2.0 1.9 NS DS SWH 5208.333 Hz 0.158946 Hz 3.1457281 sec 64 96.000 usec FIDRES AQ RG DW DE 25.61 usec 298.0 K 1.50000000 sec 1 TE D1 TDO CHANNEL f1 =-- 1H 11.38 usec -2.50 dB 18.35869598 W 400.1320007 MH2 ===== =- NUC1 P1 PL1 PL1W SFO1 F2 - Processing parameterS 32768 400.1300065 MHz SI SF WDW EM SB LB 0.30 Hz GB PC 1.00 11 10 8 7 6 5 4 3 2 1 ppm 000' 2.32 1.044 -2.08 88:I 98:T/ 1.85 1.70 1.70 69'I 89
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