Organic Chemistry  Correct Separation Scheme * cannot be hand drawn *see attached image of "incorrect separation scheme" Illustrate a correct separation scheme to isolate your molecule (2,6-dimethyloct-2-ene) from the provided second molecule. Make sure to indicate the phase of each chemical in every step (s, l, g, aq) and write the separation technique used in each step (ie: vacuum filtration).  The list below gives the reagents available in the lab.  Use any of the reagents below to isolate the compounds. Remember that the simplest separation scheme is the best one.  Try to avoid unnecessary steps.  ·   10% aqueous NaOH ·  H2O ·  5% aqueous NaHCO3 · H3PO4 ·   6M HCl · anhydrous Na2SO4 · 5% HCl · anhydrous MgSO4 ·  Diethyl ether (ether) ·  Saturated NaCl · CH3OH · Sodium borohydride (NaBH4) · lithium aluminum hydride (LiAlH4) ·  NaCl solid

Introduction to General, Organic and Biochemistry
11th Edition
ISBN:9781285869759
Author:Frederick A. Bettelheim, William H. Brown, Mary K. Campbell, Shawn O. Farrell, Omar Torres
Publisher:Frederick A. Bettelheim, William H. Brown, Mary K. Campbell, Shawn O. Farrell, Omar Torres
Chapter5: Gases, Liquids, And Solids
Section: Chapter Questions
Problem 5.104P
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Organic Chemistry 

Correct Separation Scheme

* cannot be hand drawn

*see attached image of "incorrect separation scheme"


Illustrate a correct separation scheme to isolate your molecule (2,6-dimethyloct-2-ene) from the provided second molecule. Make sure to indicate the phase of each chemical in every step (s, l, g, aq) and write the separation technique used in each step (ie: vacuum filtration).  The list below gives the reagents available in the lab.  Use any of the reagents below to isolate the compounds. Remember that the simplest separation scheme is the best one.  Try to avoid unnecessary steps. 

·   10% aqueous NaOH

·  H2O

·  5% aqueous NaHCO3

· H3PO4

·   6M HCl

· anhydrous Na2SO4

· 5% HCl

· anhydrous MgSO4

·  Diethyl ether (ether)

·  Saturated NaCl

· CH3OH

· Sodium borohydride (NaBH4)

· lithium aluminum hydride (LiAlH4)

·  NaCl solid

Incorrect Separation Scheme
S
aq
بلند سلوم
OH
OH
aq
6M HCl, vac. filtration
NaCl
ether, 10% NaHCO3
S
Na₂SO4 10H₂0
ether
OH
Na₂SO4, filtration
g
ether
ether
OH
OH
evap. ether
S
OH
OH
Transcribed Image Text:Incorrect Separation Scheme S aq بلند سلوم OH OH aq 6M HCl, vac. filtration NaCl ether, 10% NaHCO3 S Na₂SO4 10H₂0 ether OH Na₂SO4, filtration g ether ether OH OH evap. ether S OH OH
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