Part B. Identification of Mobile Phase for Separation of Acetanilide and Benzoic Acid Sketch your TLC plates. As before, measure all distances on the actual TLC plates, then record them on or adjacent to each sketch. 100% Pet. ether Std. Acetanilide R Std. Benzoic acid R O Mixture: Acetanilide R O Benzoic acid R 6 0 BC 100% ethyl acetate Std. Acetanilide R 040 Std. Benzoic acid R 0.57 3.1 (m Mixture: Acetanilide R 0-36 Benzoic acid R 0.59 7.69 cm A 44cm 14.50 28cm 50% Pet. ether / 50% ethyl acetate Std. Acetanilide R 0-20 Std. Benzoic acid R 047 Mixture: Acetanilide R 0.17 Benzoic acid R 0.44 7.5 CT 1.5cm A B 3.5cm 703 A- Acetanilide B-Benzoic Acid C-Acetanilid/Benzoic Which mobile phase provides the best overall results for the separation of acetanilide and benzoic acid? Explain why. 33cm 13 cm 7.5 cm
Part B. Identification of Mobile Phase for Separation of Acetanilide and Benzoic Acid Sketch your TLC plates. As before, measure all distances on the actual TLC plates, then record them on or adjacent to each sketch. 100% Pet. ether Std. Acetanilide R Std. Benzoic acid R O Mixture: Acetanilide R O Benzoic acid R 6 0 BC 100% ethyl acetate Std. Acetanilide R 040 Std. Benzoic acid R 0.57 3.1 (m Mixture: Acetanilide R 0-36 Benzoic acid R 0.59 7.69 cm A 44cm 14.50 28cm 50% Pet. ether / 50% ethyl acetate Std. Acetanilide R 0-20 Std. Benzoic acid R 047 Mixture: Acetanilide R 0.17 Benzoic acid R 0.44 7.5 CT 1.5cm A B 3.5cm 703 A- Acetanilide B-Benzoic Acid C-Acetanilid/Benzoic Which mobile phase provides the best overall results for the separation of acetanilide and benzoic acid? Explain why. 33cm 13 cm 7.5 cm
Chapter33: High-performance Liquid Chromatography
Section: Chapter Questions
Problem 33.15QAP
Related questions
Question
Chemistry
Would the answer to this question on the bottom be 100% Pet. ether? if so, why? if not, why not and which one is the best mobile phase and why?
Expert Solution
This question has been solved!
Explore an expertly crafted, step-by-step solution for a thorough understanding of key concepts.
Step by step
Solved in 3 steps
Knowledge Booster
Learn more about
Need a deep-dive on the concept behind this application? Look no further. Learn more about this topic, chemistry and related others by exploring similar questions and additional content below.Recommended textbooks for you
EBK A SMALL SCALE APPROACH TO ORGANIC L
Chemistry
ISBN:
9781305446021
Author:
Lampman
Publisher:
CENGAGE LEARNING - CONSIGNMENT
EBK A SMALL SCALE APPROACH TO ORGANIC L
Chemistry
ISBN:
9781305446021
Author:
Lampman
Publisher:
CENGAGE LEARNING - CONSIGNMENT