Please assign the proton peaks directly on the molecule from the NMR provided

Appl Of Ms Excel In Analytical Chemistry
2nd Edition
ISBN:9781285686691
Author:Crouch
Publisher:Crouch
Chapter14: Chromatography
Section: Chapter Questions
Problem 9P
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Please assign the proton peaks directly on the molecule from the NMR provided

SH7407.10.fid
-8.26
-8.22
8.07
-8.09
7.66
7.63
-7.62
-7.55
-7.44
-7.42
-741
-7.41
-7.39
-7.39
7.37
-7.37
7.34
7.31
11
10²7-
S
1.00
0.10
97
7.26
7.18
7.13
26.9-
19
-6.85
6.81
6.64
766
DCM impority.
9.5 9.0 8.5 8.0 7.5 7.0 6.5
6.0
-5.31
H
0.17-
H
H
5.5 5.0 4.5
f1 (ppm)
H
mm
V
-
H
H
0.15-
H
H
acetone
impurity
-NO₂
H
4.0 3.5 3.0
1.54
1.35
de-t
1.28
PAS
2.5 2.0 1.5
H₂0 impurity
1.0
-750
-700
-650
-600
-550
-500
450
-400
-350
-300
-250
-200
-150
-100
-50
-0
0.5 0.0
50
Transcribed Image Text:SH7407.10.fid -8.26 -8.22 8.07 -8.09 7.66 7.63 -7.62 -7.55 -7.44 -7.42 -741 -7.41 -7.39 -7.39 7.37 -7.37 7.34 7.31 11 10²7- S 1.00 0.10 97 7.26 7.18 7.13 26.9- 19 -6.85 6.81 6.64 766 DCM impority. 9.5 9.0 8.5 8.0 7.5 7.0 6.5 6.0 -5.31 H 0.17- H H 5.5 5.0 4.5 f1 (ppm) H mm V - H H 0.15- H H acetone impurity -NO₂ H 4.0 3.5 3.0 1.54 1.35 de-t 1.28 PAS 2.5 2.0 1.5 H₂0 impurity 1.0 -750 -700 -650 -600 -550 -500 450 -400 -350 -300 -250 -200 -150 -100 -50 -0 0.5 0.0 50
Expert Solution
Step 1

H1 NMR provides us the details regarding the structure of the molecules

The name of the given compound is 1-nitro-4-styrylbenzene

To assign the proton peaks.

steps

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