The amounts reported for the monitored ingredients under internal standard calibration are insensitive to illegal dilutions performed to the preparations, once the internal standard substance was in. True False
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The amounts reported for the monitored ingredients under internal standard calibration are insensitive to illegal dilutions performed to the preparations, once the internal standard substance was in.
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- Calculate the Constant Weight (in grams) of the Empty Crucibles. Show your solution. Crucible No. 1 2 3 Weighing 1 22.6035 22.0223 24.1535 Weighing 2 22.6017 22.0204 24.1533 Weighing 3 22.5994 22.0199 - Weighing 4 22.5992 - - Constant Weight, g ??? ??? ???Using the percent purity calculations, determine the percent yield of synthesis of aspirin. Part I Synthesis of Aspirin Mass of salicylic acid used (g) 2.029g Volume of acetic anhydride used (mL) 5ml Mass of acetic anhydride used (vol. × 1.08 g/mL) 5.4g Mass of aspirin synthesized (g) 3.256g Part II Melting Temperature Data Melting temperature (°C) 133°C Part III Salicylic Acid Standard Stock Solution Initial mass of salicylic acid (g) 0.210g Moles of salicylic acid (mol) 0.0147 mol Initial molarity of salicylic acid (M) 0.724 M Part III Beer’s Law Data for Salicylic Acid Standard Solutions Trial Concentration (M) Absorbance Water (mL) 1 10 0.301 0 2 7.5 0.219 2.5 3 5.0 0.163 5.0 4 2.5 0.074 7.5 Best-fit line equation for the salicylic acid standards Test of the Purity of the Synthesized Aspirin Initial mass of aliquot of product (g)…Make a schematic diagram for the procedure below: A. Constant weighing of the crucibles Bring two porcelain crucibles to constant weight by heating to redness for 15 min over a burner (not including the cover; see Figure 1 for heating set-up). Cool the crucibles briefly on clean Al foil-covered wire gauze at room temperature for 5 min and into the desiccator for 25 minutes. Weigh each crucible accurately on an analytical balance. Repeat procedure a and b until two successive weights agree within ± 0.3 mg, be sure that all oxidizable substances on the entire surface of each crucible have been burned off.
- After the extraction process, the organic solvent containing the organic compound was cooled and filtered after the crystals appeared. Upon filtration, the filter paper with the crystals are weighed immediately. Assume there were no additional steps in between and after, what are the possible errors committed in this set up?Choose the one correct or one incorrect statement regarding filtration: gravity filtration uses a Buchner funnel, filtering flask and negative pressure filter paper should be wet with solvent to seal it to the funnel before filtering the solution collected in the filtering flask is called the residue vacuum filtration is most often used to remove impurities from a solution the solution to be filtered should completely fill the top of a Buchner funnelAmylum, commonly known as starch is a white powder with variable molecular formula due to the different number of repeating sugar units based on the plant that it is obtained from. A sample of amylum in the form of spherical beads was subjected to series of analyses to determine physicochemical properties in the quality control unit of a factory. From the results each bead is found to have a 4.5 mL volume and 1.47 g/mL density. 4 of the beads were placed in a reaction chamber combusted, as a result, 43.1 g CO2 and 14.7 g H2O were obtained. If the molecular weight of the amylum is 972.84 g/mol how many repeating units the starch molecule consist and what is the molecular formula of the starch? [Empirical Formula=CxHyOz, Repeating unit=n, Molecular Formula=( CxHyOz)*n= CnxHnyOnz]
- What is the purpose of the internal calibration mass at the upper left in the electronic balanceA student obtained 2.111 g of a mixture containing four components. After performing separation by chemical and physical methods, the student obtained the following mass data: Component 1: 0.486 g Component 2: 0.317 g Component 3: 0.127 g Component 4: 0.929 g Calculate the total percent recovery of the mixture. (Please show work)I got a task in analytical chemistry to calibrate, standardize, verify and validate an analytical balances
- Silver nitrate can be purchased as high purity grade and does not require to undergo standardization against a secondary standard. True False1. Explain the importance of using a thermometer in the simple distillation setup? 2. Enumerate the characteristics of a substance for it to be separated from the heterogeneous mixture by steam distillation? Please explain well and don't copy from googleThe density of the first fraction collected would be expected to be close to a value of ______. 1.00 g./mL 0.895 g/mL 0.789 mL 0.950 g.mL