To compensate for a complex or unknown matrix, the ● ● A. Calibration curve B. Standard addition Method C. Internal Standard Method D. Dilution method E. Least-Squares Analysis F. Standardization method should be used to determine the analyte concentration
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- 10-mL aliquots of an environmental water sample were pipetted into five 50.00-mL volumetric flasks. Exactly 0.00, 5.00, 10.00, 15.00, and 20.00-mL of a standard solution containing 11.1 ppm Fe3+ were added to each, followed by an excess of thiocyanate ion to give the red complex Fe(SCN)2+. After dilution to volume, the instrumental response for each of the five solutions measured with a colorimeter was found to be 0.240, 0.437, 0.621, 0.809, 1.809, respectively. Using Excel and the LINEST function, what was the concentration in the water sample (including error)? [HINT: consider the type of calibration scheme used.]The buret was filled with 0.100 M HCl solution. Then was transferred in a 25.0 mL of saturated calcium hydroxide solution (2g of calcium hydroxide per 100 ml of water) in two separate E-flasks. Then 2 drops of phenolphthalein was added to each flask Titration data for the determination of the common ion effect: Trial 1: Final Buret reading (ml)-29.50; Initial Buret reading (ml)- 26.10; Temperature (Celcius)- 25 Trial 2: Final Buret reading (ml)-33.30; Initial Buret reading (ml)- 29.50; Temperature (Celcius)- 25 Voume of HCl used: Trial 1- 3.40ml; Trial 2- 3.80mL. Report in proper sigfigs. 1. Compute for the moles of H+ used and the moles of OH- present. moles of H+ used = (concentration of HCl) × (volume of HCl used)moles of OH- = moles of H+ used 2. Use the dilution formula to determine the initial concentration of the common ion. C1V1 = C2V2 3. Construct an ICE table for the reaction.4. Calculate the molar solubility…A 25.0 cm portion of 0.200, mol dm^-3 sodium ethanedioate solution was warmed and titrated against a solution of potassium manganate(VII). If 17.2 cm^3 of potassium manganate(VII) are required, what is its concentration?
- What conclusion can be derived from the following sentences regarding analytical methods: I. Classical methods (gravimetry and volumetric methods) are no longer useful in analytical chemistry. II. Volumetric methods do not require calibration if a primary standard is used as titrant. III. Instrumental methods are useful with analyte solutions that are less than 1.00 mM. IV. Classical methods yield high precision and accuracy at concentrations greater than 1.00 mM. What conclusion can be derived from the following sentences regarding analytical methods: Two statements are incorrect. All statements are correct. One statement is incorrect. Only one statement is correct. All statements are incorrect.The buret was filled with 0.100 M HCl solution. Then was transferred in a 25.0 mL of saturated calcium hydroxide solution (2g of calcium hydroxide per 100 ml of water) in two separate E-flasks. Then 2 drops of phenolphthalein was added to each flask Titration data for the determination of the common ion effect: Trial 2: Final Buret reading (ml)-33.30; Initial Buret reading (ml)- 29.50; Temperature (Celcius)- 25 Voume of HCl used: Trial 2- 3.80mL. Report in proper sigfigs. 1. Compute for the moles of H+ used and the moles of OH- present. moles of H+ used = (concentration of HCl) × (volume of HCl used)moles of OH- = moles of H+ used 2. Use the dilution formula to determine the initial concentration of the common ion. C1V1 = C2V2 3. Construct an ICE table for the reaction.4. Calculate the molar solubility (in mol/L) of OH- and Ca2+.5. Determine the solubility of Ca(OH)2 in g/L. (MM of Ca(OH)2 = 74.096 g/mol).…The buret was filled with 0.100 M HCl solution. Then was transferred in a 25.0 mL of saturated calcium hydroxide solution (2g of calcium hydroxide per 100 ml of water) in two separate E-flasks. Then 2 drops of phenolphthalein was added to each flask Titration data for the determination of the common ion effect: Trial 2: Final Buret reading (ml)-33.30; Initial Buret reading (ml)- 29.50; Temperature (Celcius)- 25 Voume of HCl used: Trial 2- 3.80mL. Report in proper sigfigs. 1. Calculate the molar solubility (in mol/L) of OH- and Ca2+.2. Determine the solubility of Ca(OH)2 in g/L. (MM of Ca(OH)2 = 74.096 g/mol). 3. Calculate the Ksp of Ca(OH)2. Make sure to include the effect of the common ion in the calculation.
- Which of the following is TRUE regarding instrumental methods of analysis? A. these methods have lower throughput compared to classical method. B. these methods have lower accuracy compared to classical methods. C. these methods can measure lower analyte concentration than classical methods D. these methods have higher precision compared to classical methods.A method for the analysis of Ca2+ in water suffers from an interference in the presence of Zn2+. When the concentration of Ca2+ is 100 times greater than that of Zn2+, an analysis for Ca2+ gives a relative error of +0.5%. What is the selectivity coefficient for this method?An automatic titration was performed with the following results: Standardized NaOH Solution Concentration: 0.1191 M Volume of HA- product examined in each trial: 25.00 mL Volume of Standardized NaOH Titrant used to achieve the first equivalence point: Trial #1: 1.300 mL Trial #2: 1.137 mL Trial #3: 1.140 mL Calculate the %(w/v) for each trial, Average Concetration (%), Deviation (%), Standard Deviation (%), and RSD (%)
- When using ion-selective electrodes, to comensate for a complex or unknown matrix, the __________ method can be used to determine the analyte concentration. a) least-squares analysis b) standardization c)standard addition d)dilution e)calibration curve60 ml of standard hardness containing 1 mg of pure CaCO3 per ml consumed 22 ml of EDTA. 40 ml of water sample consumed 20 ml of EDTA solution using EBT indicator. 40 ml of water sample after boiling, filtering consumed 15 ml of EDTA. Calculate the temporary and permanent hardness of water sample.Does KMNO4 oxidize or reduce an analyte during permanganimetry?