Which of the following is the correct flow of the mobile phase in HPLC? Solvent degasser>Guard Column>Detector>Waste Bottle Solvent degasser>Detector>Guard Column>Waste Bottle Solvent degasser pressure pump>gradient valve>Waste Bottle gradient valve solvent degasser pressure pump>Waste Bottle
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- In using ATR-FTIR, liquid samples need no additional pressure because it is always in optimal contact. True FalseWhich part of the GC equipment does separation takes place?Various parameters in a gas absorption experiment are as follows; Water flow rate =5 L/min, Air flow rate=25 L/min, CO2 flow rate=6 L/min. Then, to find the amount of CO2 absorbed into the water 1 hour after the system is started and stabilized, 50 mL samples are taken from the inlet and outlet of the tank and titrated with 0.01M NaOH. 100mL samples are taken from the tower entrance and exit and sent to the hemp apparatus. The consumptions measured with the help of the Hemp apparatus are 2.1 mL (inlet) and 1.9 mL (output), respectively. According to this, find the amount of CO2 absorbed by titration? (Note: The relative error in the experiment is 10.)
- Gas chromatography was used to analyse for residues of toxic solvents, including benzene and 1,2-dichloroethane (DCE), in a pharmaceutical preparation. The following conditions were used: Column: 30 m long capillary with polysiloxane stationary phaseCarrier gas: He at 35 cm s–1 constant flowOven program: 40 °C at t = 0, increasing at 10 °C min–1 to 240 °C at t = 20 min. Detector: flame ionisation (FID) Benzene eluted with retention time = 11.5 min, peak width = 0.26 min 1,2-dichloroethane (DCE) eluted with retention time = 11.8 min, peak width = 0.28 min (i) What are the strengths and limitations of the flame ionisation detector in this application, compared with other possible methods of detection? (ii) What is the resolution, RS, for the separation of benzene and DCE on this column? (iii) Suggest two ways by which the resolution of benzene and DCE might be improved. Explain your choices.A solution containing 100 lbm KNO 3/100 lbm H 2O at 80°C is fed to a cooling crystallizer operated at 25°C. Slurry from the crystallizer (KNO3 crystals suspended in saturated solution) is fed to a filter, where the crystals are separated from the solution. Use the solubility data in Figure 6.5-1 to determine the production rate of crystals (lbm/lbm feed) and the solid-to-liquid mass ratio (lbm crystals/lbm liquid) in the slurry leaving the crystallizer.Which statement justifies the need for a high molecular mass primary standard or reagent? It reduces changes in mass in dry environment It reduce the error from mass measurement It increases the ratio of surface to particle interaction It strongly adsorbs water avoiding moisture factor
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