You have measured the blank for a determination of arsenic in food samples by hydride-generation atomic fluorescence spectrometry. The blank values are: 0.23 ppb, 0.14 ppb, 0.16 ppb, 0.28 ppb, 0.18 ppb, 0.09 ppb, 0.10 ppb, 0.20 ppb, 0.15 ppb, 0.21 ppb As. What is the LOD?

Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter15: Molecular Luminescence Spectrometry
Section: Chapter Questions
Problem 15.6QAP
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You have measured the blank for a determination of arsenic in food samples by hydride-generation atomic fluorescence spectrometry. The blank values are: 0.23 ppb, 0.14 ppb, 0.16 ppb, 0.28 ppb, 0.18 ppb, 0.09 ppb, 0.10 ppb, 0.20 ppb, 0.15 ppb, 0.21 ppb As. What is the LOD?

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Step 1

Given,

Sr. No. (N) 1 2 3 4 5 6 7 8 9 10
Blank values(ppb) 0.23 0.14 0.16 0.28 0.18 0.09 0.10 0.20 0.15 0.21

Limit of detection (LOD)=?

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