1(a) Base on the information provided, determine the structures of compounds. (b) Assign all peaks in 'H and "C NMR spectra of compounds

Organic Chemistry: A Guided Inquiry
2nd Edition
ISBN:9780618974122
Author:Andrei Straumanis
Publisher:Andrei Straumanis
ChapterL4: Proton (1h) Nmr Spectroscopy
Section: Chapter Questions
Problem 24CTQ
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13C NMR Spectrum
(100.0 MHz, CDCI, solution)
DEPT
solvent
proton decoupled
200
160
120
80
40
O 8 (ppm)
H NMR Spectrum
(400 MHz. CDCI, solution)
Exchanges
with Oyo
еxpansion
2H
2H
1H
2H
2H
TMS
2.5
2.0
1.5
10
4
3 2
1
8 (ppm)
Transcribed Image Text:13C NMR Spectrum (100.0 MHz, CDCI, solution) DEPT solvent proton decoupled 200 160 120 80 40 O 8 (ppm) H NMR Spectrum (400 MHz. CDCI, solution) Exchanges with Oyo еxpansion 2H 2H 1H 2H 2H TMS 2.5 2.0 1.5 10 4 3 2 1 8 (ppm)
Instruction:
1(a) Base on the information provided, determine the structures of compounds.
(b) Assign all peaks in 'H and "C NMR spectra of compounds
Compound 1:
2114
3295
IR Spectrum
(liquid film)
4000
3000
2000
1600
1200
800
V (cm")
100
Mass Spectrum
82
80
60
20
M*- 83
CgHgN
40
80
120
160
200
240
280
m/e
yeed eseg jo%
Transcribed Image Text:Instruction: 1(a) Base on the information provided, determine the structures of compounds. (b) Assign all peaks in 'H and "C NMR spectra of compounds Compound 1: 2114 3295 IR Spectrum (liquid film) 4000 3000 2000 1600 1200 800 V (cm") 100 Mass Spectrum 82 80 60 20 M*- 83 CgHgN 40 80 120 160 200 240 280 m/e yeed eseg jo%
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