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- Explain how to obtain larger particles based on the relative supersaturationBriefly compare the advantages and disadvantages of Nujol mulls and KBr pellets for the analysis of solid samples by IR spectrometry.What are the necessary conditions for a metal isotope to be useful as a sources in mossbauer spectroscopy.
- CIE standardized instruments of the geometry of 45。 / 0。and d/8。are widely applied for colour analysis of food samples. (a.) With the aid of diagrams, explain how the measurement is achieved using these two geometries. (b.) Which of the geometries is more preferred in a colour analysis of food samples? Explain your answer briefly.1. Discuss the importance and precautions in using glass cuvettes. 2. Explain in your own understanding the principles of UV-Vis Spectrometer.Discuss the origins of the local, neighbouring group, and solvent contributions to the shielding constant.
- Seawater was spiked with phosphate to achieve a quantifiable range of phosphate concentrations by spectroscopy. What components of the spectrophotometer or sample preparation could be changed that would improve detection limits?1. Define: spectrochemical methods, spectroscopy, spectrometry, spectrometer, and spectrophotometer. 2. What is specific about the general analytical strategy for spectrochemical analysis methods comparedto instrumental analysis in general? 3. What is meant by the dual nature of light?Discuss the advantages, disadvantages, and limitations of the technique of cyclic voltammetry in both qualitative and quantitative measurements.
- The emission of quinine is observed to increase as the pH increases from pH 2.5 to 3.75 but is then observed to decrease at pH > 3.75. Suggest what may be happening to the molecule to account for this observation. Comment on the concentration of quinine in terms of EU limits.Describe the units of IR in relation to frequency and energy and describe the functions of an FT-IR spectrometer.Lead is determined by atomic absorption at 283.3 nm, whereas it is determined at 405.8 nm by flame emission. Explain why the most sensitive line is different for these two methods.