2. A Tlc plate was run on the fractions (#1-4) collected from a silica gravity column chromatography that was done. The Tlc plate was developed in 20% ethyl acetate/80% hexanes and is shown below. -------- Fraction # 1234 The compounds that were isolated in each fraction are shown below. Label each compound with the number of the fraction that it was likely found in, based on the TLC results. For example, was compound A found in fraction #2? If so, write A = #2 fraction. Do the same for all 4 compounds. CH₂CH₂ .CH3 OH og OH D B CH₂

EBK A SMALL SCALE APPROACH TO ORGANIC L
4th Edition
ISBN:9781305446021
Author:Lampman
Publisher:Lampman
Chapter88: Column Chromatography
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2. A Tlc plate was run on the fractions (#1-4) collected from a silica gravity column chromatography that
was done. The Tlc plate was developed in 20% ethyl acetate/80% hexanes and is shown below.
--------
Fraction #
1234
The compounds that were isolated in each fraction are shown below. Label each compound with the
number of the fraction that it was likely found in, based on the TLC results. For example, was compound
A found in fraction #2? If so, write A = #2 fraction. Do the same for all 4 compounds.
CH₂CH3
.CH3
OH
og
OH
D
B
CH₂
Transcribed Image Text:2. A Tlc plate was run on the fractions (#1-4) collected from a silica gravity column chromatography that was done. The Tlc plate was developed in 20% ethyl acetate/80% hexanes and is shown below. -------- Fraction # 1234 The compounds that were isolated in each fraction are shown below. Label each compound with the number of the fraction that it was likely found in, based on the TLC results. For example, was compound A found in fraction #2? If so, write A = #2 fraction. Do the same for all 4 compounds. CH₂CH3 .CH3 OH og OH D B CH₂
3. Complete the acid-base reaction below by writing the product(s).
NH₂
+ HCI
aniline
Indicate the solubility of aniline and its conjugate acid in diethyl ether and water.
Transcribed Image Text:3. Complete the acid-base reaction below by writing the product(s). NH₂ + HCI aniline Indicate the solubility of aniline and its conjugate acid in diethyl ether and water.
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