2. The goal behind suction filtration is to remove soluble impurities that are on the surface of the crystals. Therefore, why can't you simply use suction filtration instead of recrystallization to purify an impure solid?
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A: As per bartleby guidelines I answered only first question so please don't mind.Thanks in advance.
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- 1. Explain the importance of using a thermometer in the simple distillation setup? 2. Enumerate the characteristics of a substance for it to be separated from the heterogeneous mixture by steam distillation? Please explain well and don't copy from googleIn recrystallization, fluted filter paper is used instead of a regular cone because it minimizes its contact with the glass funnel. Why is this important?Volumetric pipettes are designed to deliver a precise amount of liquid, but only if you a. submerge the end of the pipette into a solution you are delivering. b. allow the pipette to drain freely, and leave any residual solution in the pipette. c. hold the pipette at a 45 degree angle and ensure that all the liquid is delivered.
- Based on the melting point of your impure solid, you look at the given samples and believe you havecompound A. Compound A is recrystallized using a mixed solvent system of ethanol and water. You add1 ml of hot ethanol to your sample and it doesn’t completely dissolve. You continue to add hot ethanolbut there isn’t any change. Some solid remains. What should you do next?We separated a mixture of sodium carbonate and calcium chloride using Gravity Filtration. Additionally, did vacuum filtration for crystallized Vannilin. However we were not able to recover 100% of the original sample the question is: what do you think are the factors that contribute to low percentage recovery?1. How to collect main batch of crystals using vacuum filtration (Set-up, things to remember)• Why use small amounts of cold water for washing? What is being washed away (2things)?2. Why measure the volume of mother liquor in a graduated cylinder?3. How to let the main batch of crystals dry/how will they be stored until next week?4. How to collect the small amount of crystals from step 4 (those that were not subjected tocrystallization)• What can we expect of this small batch of crystals compared to the main batch?
- DATA Note: Use the videos as references except when data is provided here. Table 1. Selection of Recrystallizing Solvent. Solvents Dissolution at room temperature? (+ or −) Dissolution at elevated temperature? (+ or −) Distilled water - - Acetone + n/a 95% ethanol - + Toluene + n/a Solid sample: Naphthalene Table 2. Mass Measurements. Mass, g Sample solid 0.5021 Empty watch glass 35.7602 Watch glass with recrystallized sample 36.2485 Table 3. Melting Point Determination. Temperature, oC Appearance of Sample in Capillary Tube … Solid 78.4 Solid 79.3 Solid with signs of liquid 79.9 Solid, liquid 80.6 Liquid, solid 81.3 Liquid with signs of solid … Liquid Theoretical Melting Point, oC: 80.2°C (176.4°F) QUESTIONS Which solvent should be used as the recrystallizing solvent? Check if your chosen solvent satisfies all characteristics of a good…In paper chromatography, the stationary phase is made of ---------- and the mobile phae is made of ----------- a) liquid, liquid b) liquid, gas c) solid, gas d) solid, liquidHow can you tell that a compound is impure? (or pure?) What are the characteristics considered when taking a melting point? What is recrystallization? What is happening on a molecular level (videos are provided) How are solvents chosen for recrystallization? (single solvent or mixed-solvent system).What are the properties of a good solvent system? How are crystals collected?
- In which of the following scenarios might you expect the observed melting point to be depressed? Choose all that apply. a. The heating rate for measuring the melting point was set too high. b. The percent recovery of recrystallized solid was less than 100%. c. A solid that was recrystallized from hexane was filtered and dried without washing with additional hexane while it was on the filter funnel. d. A solid recrystallized from toluene was left on the filter funnel for only a short time before its melting point was measured. e. The melting point capillary tube was packed with too much material.In vacuum filtration, the filter paper should be wet before the final product solution is poured into the buchner funnel. Explain why such an action should be implemented.Filter paper is usually a poor material on which to powder a solid sample before introducing it into a capillary melting-point tube because small particles of paper may end up in the tube along with the sample. Why is this undesirable? and how might the presence of paper in the sample make the melting-point determination difficult