4000 100 38898 IR Spectrum (liquid film) 80 MMMMM % of base peak 10 3000 43 40 13C NMR Spectrum (50 0 MHz. CDCI, solution) 5.5 59 9 87 DEPT CH₂ CH₂ CH proton decoupled 200 ¹H NMR Spectrum (200 MHz, CDCI, solution) expansions 80 2.5 45 ppm 8 nm homm 1747 1200 800 1600 v (cm'¹) Mass Spectrum M 146 C6H1004 120 160 m/e 2000 160 7 200 240 280 solvent 120 15 ppm 6 5 80 4 3 40 Problem 47 No significant UV absorption above 220 nm 2 0 8 (ppm) 1 0 8 (ppm)

4000 100 38898 IR Spectrum (liquid film) 80 MMMMM % of base peak 10 3000 43 40 13C NMR Spectrum (50 0 MHz. CDCI, solution) 5.5 59 9 87 DEPT CH₂ CH₂ CH proton decoupled 200 ¹H NMR Spectrum (200 MHz, CDCI, solution) expansions 80 2.5 45 ppm 8 nm homm 1747 1200 800 1600 v (cm'¹) Mass Spectrum M 146 C6H1004 120 160 m/e 2000 160 7 200 240 280 solvent 120 15 ppm 6 5 80 4 3 40 Problem 47 No significant UV absorption above 220 nm 2 0 8 (ppm) 1 0 8 (ppm)

Fundamentals Of Analytical Chemistry

9th Edition

ISBN:9781285640686

Author:Skoog

Publisher:Skoog

Chapter33: High-performance Liquid Chromatography

Section: Chapter Questions

Problem 33.14QAP

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