A wittig reaction experiment: Week 1 -》 preparation of phosphonium salt  Materials : triphenylphosphine (5.3g),methyl Bromoacetate 3.36g (2.1ml)  , ethanol 30ml . The yield obtained was 8.93g . Calculate the percentage yield

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A wittig reaction experiment:

Week 1 -》 preparation of phosphonium salt 

Materials : triphenylphosphine (5.3g),methyl Bromoacetate 3.36g (2.1ml)  , ethanol 30ml . The yield obtained was 8.93g .

Calculate the percentage yield 

 

Week 2 -》 Formation of the tlide and wittig reaction 

Materials :Phosphonium salt  (5g),  napthyl-2- carboxwaldehyde( 2.65g), 20 ml of water and 5 nl of Nahco3.

Yield obtained was 0.51g .Calculate the percentage yield

 

Week 3: Solvent free wittig reaction 

Materials: Benzyltriphenylphosphonium chloride (0.5g ), 4 - Bromoabenzaldehyde (0.24g), Potassium phosphate (tribasi c) 0.275g .The yield obtained was 1.21g. Calculate the  percentage yield 

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