Analyze the effects caused by various impurities on precipitate during the gravimetric analysis and suggest the measures to reduce the impact of these impurities.
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Analyze the effects caused by various impurities on precipitate during
the gravimetric analysis and suggest the measures to reduce the impact
of these impurities.
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- Enumerate at least two important things to do to maximize yield when using vacuum filtration in the synthesis of aspirin.Why a precipitate of manganese dioxide be removed from the potassium permaganate solution before standardization?in a chromatographic analysis of water from a drinking fountain gives area of 1.56*10^4, 5.12*10^4, 1.49*10^4 and 1.76*10^4 for CH3CL3, CHCL2BR, CHCLBR2 and CHBR3 respectively. determine the percentage concentration of each of the triichoromethane in the sample
- Briefly explain how slow cooling contributes to the formation of pure crystals during recrystallization.In gravimetric analysis, co-precipitation occurs alongside with analyte precipitation,resulting in the introduction of impurity and excess mass. Occlusion and inclusion areamong the sources of impurities. Distinguish the difference between occlusion andinclusion and compare them using diagramsIs there a difference when the needle or metal clip is placed on the surface of distilled water with dilute amounts of liquid detergent? Explain your observations in terms of the strength of IMFA present in each condition.
- The analgesic aspirin is soluble at 25oC in water to the extent of 3mg/mL and in ethylacetate to the extent of 86 mg/mL. The approximate distribution coefficient of aspirin in these two solvents is __Write an objective of separation of a mixture by extractionIf 30.0 mL of water that is 0.0500 M in Q is to be extracted with four 10.0 mL portions ofan immiscible organic solvent, what is the minimum distribution coefficient that allowstransfer of all but 1.00 x 10–4 of the solute to the organic layer.