Briefly explain method validation in analytical chemistry? Discuss typical validation characteristics which could be considered. Name some international organisations offering guidelines on method validation
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- What is the actual or real-life application of precipitation gravimetric analysis? Include the specific methodology.2 what is the purpose of BSC Level 1 & 2, proper layout, performance, and its application in biosafety assessmentHere is a use objective for a chemical analysis to be performed at a drinking water purification plant: “Data and results collected quarterly shall be used to determine whether the concentrations of haloacetates in the treated water demonstrate compliance with the levels set by the Stage 1 Disinfection By-products Rule using Method 552.2” (a specification that sets precision, accuracy, and other requirements). Which one of the following questions best summarizes the meaning of the use objective?(i) Are haloacetate concentrations known within specified precision and accuracy?(ii) Are any haloacetates detectable in the water?(iii) Do any haloacetate concentrations exceed the regulatory limit?
- What application of CHNS elemental analysers can be suggested in Food Analysis Give examples for it and explain its importanceThe researcher extracts a sample of well water and prepares it for TXRF analysis with a 10.00 mg/L V internal standard, like the calibration standards. The result produces SCa = 69297.81 and SV = 13481.2.Determine the concentration of Ca.Structural elucidation of a sample component is possible through point estimation of its components with modern instrumentation methodologies. Additionally, characterization of their chemical nature is possible through qualitative analytical methods. A - If the first statement is TRUE and the second statement is FALSEB - If the first statement is FALSE and the second statement is TRUEC - If both statements are TRUED - If both statements are FALSE
- The student was supposed to measure the pH of a 0.1 M hydrochloric acid solution. For this purpose, he used a pH-meter and obtained the following results: 0.90, 0.93, 1.04, 1.02. Present the appropriate graphic and statistical elaboration of the performed analysis and confirm whether the applied pH-meter worked properly.The partition coefficient of ammonia between water and chloroform is wanted to be determined. The necessary quantities of ingredients are taken into the separation funnel, and the extraction process is applied. At the end of the extraction process, 5 mL portions of each of the water and chloroform phases are titrated with 0.1 M HCI in the presence of methyl orange indicator. If the volumes spent at the turning points are 7.2 and 5.1 mL, respectively, calculate the KSU, KLOROFORM (Dispersion coefficient) value.What are method blanks and method detection limit used in analytical chemistry? Explain thoroughly
- a- Separation is essential in chemical analysis especially when we are dealing with complexmixture of chemical species. Name 1 separation technique based on basis of operation asbelow. Basis of operation Techniquei) Sizeii) Mass and densityiii) Change in physical stateDescribe the following as used in analytical chemistry a) semiqualitative analysis b)Assay c) derivatisationWhat is the actual or real-life application of gravimetric titrimetry? Include the specific methodology.