C. Experimental Procedure: (record Observations in notebook in ink) First Week Add 10 mL of glacial acetic acid to 5 mL of isoamyl alcohol in a 125 mL Erlenmeyer flask. (Because of the very unpleasant odor of acetic acid, dispensing of the acid and mixing with alcohol must be performed under the hood). Carefully add 3 mL of concentrated sulfuric acid (being careful not to wet the neck of the flask which will be in contact with the cork stopper), swirl the mixture, stopper tightly with a cork and store at room temperature until the next lab period. NOTE: Extreme care must be exercised in order to avoid contact with concentrated sulfuric acid. It will cause serious burns if it is spilled on the skin. If it comes in contact with the skin or clothes, it must be washed off immediately. In addition, sodium bicarbonate may be used to neutralize the acid. Clean up all spills, immediately!

C. Experimental Procedure: (record Observations in notebook in ink) First Week Add 10 mL of glacial acetic acid to 5 mL of isoamyl alcohol in a 125 mL Erlenmeyer flask. (Because of the very unpleasant odor of acetic acid, dispensing of the acid and mixing with alcohol must be performed under the hood). Carefully add 3 mL of concentrated sulfuric acid (being careful not to wet the neck of the flask which will be in contact with the cork stopper), swirl the mixture, stopper tightly with a cork and store at room temperature until the next lab period. NOTE: Extreme care must be exercised in order to avoid contact with concentrated sulfuric acid. It will cause serious burns if it is spilled on the skin. If it comes in contact with the skin or clothes, it must be washed off immediately. In addition, sodium bicarbonate may be used to neutralize the acid. Clean up all spills, immediately!

Principles of Instrumental Analysis

7th Edition

ISBN:9781305577213

Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch

Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch

Chapter26: An Introduction To Chromatographic Separations

Section: Chapter Questions

Problem 26.12QAP

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