DATA FROM RECRYSTALLIZATION EXPERIMENT Weight of crude benzoic acid, g 0.2498 Weight of filter paper, g 1.0211 Weight of filter paper with crystal, g 1.215 Weight of recrystallized benzoic acid, g % Recovery DATA FROM SUBLIMATION EXPERIMENT Weight of crude benzoic acid, g 0.1104 Weight of filter paper, g 0.9887 Weight of filter paper with crystal, g 1.0318 Weight of recrystallized benzoic acid, g % Recovery

DATA FROM RECRYSTALLIZATION EXPERIMENT Weight of crude benzoic acid, g 0.2498 Weight of filter paper, g 1.0211 Weight of filter paper with crystal, g 1.215 Weight of recrystallized benzoic acid, g % Recovery DATA FROM SUBLIMATION EXPERIMENT Weight of crude benzoic acid, g 0.1104 Weight of filter paper, g 0.9887 Weight of filter paper with crystal, g 1.0318 Weight of recrystallized benzoic acid, g % Recovery

Fundamentals Of Analytical Chemistry

9th Edition

ISBN:9781285640686

Author:Skoog

Publisher:Skoog

Chapter28: Atomic Spectroscopy

Section: Chapter Questions

Problem 28.13QAP

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Gravimetric factor:A 1.0125 g portion of the sample was oven-dried leaving 0.9385 g of dry matter. In a similar experiment a 2.0163 g portion of the sample was oven-dried and extracted with a non-polar solvent. the solvent was evaporated leaving a 0.8444 g residue. what is the amount of crude fat present in the feed? (in %w/w, dry matter basis)
10.Consider synthesis of nylon-6,10 from stoichiometric amounts of hexamethylene diamine, H2N(CH2)6NH2, and sebacic acid, HOO(CH2)8COOH. At 98% conversion of carboxylic acid groups, determine (a) Mn and Mw of the product, and (b) the sum of the mole fractions and that of the weight fractions of species containing 1 through 6 (inclusive) monomer units.
For Indirect Iodometric Analysis of Copper... ~0.0896g KIO3 necessary to consume 350mL of 0.1 M Na2S2O3, Na2S2O3 is stored in an amber glass bottle until ready for use. Primary Standard KIO3 has 2g of KI, 50mL of DI water, and 10 mL of 1.0M HCl is added then immediately titrated with Na2S2O3 until medium yellow or straw... then 5mL of starch indicator is added and titrated again until blue black color turns clear. Unknown CuO use 1.2G of Unknown, 20mL of HNO3 heated until sample dissolved, 25 mL of DI water added and boiled until clear light blue color, after cooling 1:1 NH3 added (~34.47 mL of NH4OH reagent) until permanent deep blue color amine complex, 2g of NH4HF2 added and swirled until dissolved, 3 g of KI is added then titrated immediately with Na2S2O3 until brown color of iodide is nearly gone (brown milk color), 2 g of KSCN and 3 mL of starch indicator is then added with titration continuing until disappearance of new blue black color. 1. Na2CO3 is often added to thiosulfate…
For Indirect Iodometric Analysis of Copper... ~0.0896g KIO3 necessary to consume 350mL of 0.1 M Na2S2O3, Na2S2O3 is stored in an amber glass bottle until ready for use. Primary Standard KIO3 has 2g of KI, 50mL of DI water, and 10 mL of 1.0M HCl is added then immediately titrated with Na2S2O3 until medium yellow or straw... then 5mL of starch indicator is added and titrated again until blue black color turns clear. Unknown CuO use 1.2G of Unknown, 20mL of HNO3 heated until sample dissolved, 25 mL of DI water added and boiled until clear light blue color, after cooling 1:1 NH3 added (~34.47 mL of NH4OH reagent) until permanent deep blue color amine complex, 2g of NH4HF2 added and swirled until dissolved, 3 g of KI is added then titrated immediately with Na2S2O3 until brown color of iodide is nearly gone (brown milk color), 2 g of KSCN and 3 mL of starch indicator is then added with titration continuing until disappearance of new blue black color. 4. Why is the starch indicator solution…
A sample of steel (0.506 g) was digested in acid and the solution made up to 100 cm3 with deionised water. Aliquots (25.0 cm3) of this solution were transferred into two volumetric flasks (100 cm3) labelled A and B. Flask A was made up to volume with deionised water. To flask B was added 10.0 cm3 of a 260 ppm standard solution of Mn2+ which was then also made up to volume with deionised water. The following absorbance results were obtained: Solution A = 0.356, Solution B = 0.578. Use these results to calculate the percentage (% w/w) of manganese in the steel sample.
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