Illustrate a correct separation scheme to isolate your molecule (2,6-dimethyloct-2-ene) from the provided second molecule. Make sure to indicate the phase of each chemical in every step (s, l, g, aq) and write the separation technique used in each step (ie: vacuum filtration).  The list below gives the reagents available in the lab.  Use any of the reagents below to isolate the compounds. Remember that the simplest separation scheme is the best one.  Try to avoid unnecessary steps.  ·   10% aqueous NaOH ·  H2O ·  5% aqueous NaHCO3 · H3PO4 ·   6M HCl · anhydrous Na2SO4 · 5% HCl · anhydrous MgSO4 ·  Diethyl ether (ether) ·  Saturated NaCl · CH3OH · Sodium borohydride (NaBH4) · lithium aluminum hydride (LiAlH4) ·  NaCl solid

Fundamentals Of Analytical Chemistry
9th Edition
ISBN:9781285640686
Author:Skoog
Publisher:Skoog
Chapter7: Statistical Data Treatment And Evaluation
Section: Chapter Questions
Problem 7.27QAP
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Organic Chemistry 

Correct Separation Scheme

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Illustrate a correct separation scheme to isolate your molecule (2,6-dimethyloct-2-ene) from the provided second molecule. Make sure to indicate the phase of each chemical in every step (s, l, g, aq) and write the separation technique used in each step (ie: vacuum filtration).  The list below gives the reagents available in the lab.  Use any of the reagents below to isolate the compounds. Remember that the simplest separation scheme is the best one.  Try to avoid unnecessary steps. 

·   10% aqueous NaOH

·  H2O

·  5% aqueous NaHCO3

· H3PO4

·   6M HCl

· anhydrous Na2SO4

· 5% HCl

· anhydrous MgSO4

·  Diethyl ether (ether)

·  Saturated NaCl

· CH3OH

· Sodium borohydride (NaBH4)

· lithium aluminum hydride (LiAlH4)

·  NaCl solid

Incorrect Separation Scheme
شد
S
aq
OH
OH
aq
NaCl
ether, 10% NaHCO3
6M HCl, vac. filtration
S
Na₂SO4 10H₂O
ether
OH
Na₂SO4, filtration
g
ether
ether
OH
OH
evap. ether
S
OH
OH
Transcribed Image Text:Incorrect Separation Scheme شد S aq OH OH aq NaCl ether, 10% NaHCO3 6M HCl, vac. filtration S Na₂SO4 10H₂O ether OH Na₂SO4, filtration g ether ether OH OH evap. ether S OH OH
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