Include the 'H-NMR and 1³C-NMR data for the product in separate tables with a labeled diagram 'H: chemical shift (experimental), chemical shift (literature), multiplet structure, integration, assignment 13C: chemical shift (experimental), chemical shift (literature), assignment In the current experiment, we will use a different electrophile (the tert.-butyl cation) to alkylate 1,4-dimethoxybenzene. This is a Friedel-Crafts Alkylation reaction. OCH3 (H;C),C. OCH3 (CH3),COH CH;COOH/H,SO4 H;CO H,CO C(CH3)3 Characterization IV • 13C-NMR Spectrum • Six signals from compounds and three lines from NMR solvent 8(ppm) Assignment 29.8 C(CH;); | C(CH;); OCH3 34.6 55.9 Arene-C ortho to OCH3 Arene-C attached to C(CH;); Arene-C attached to OCH; |CDCI, (three lines) 111.7 136,3 152.0 77 -1633

Include the 'H-NMR and 1³C-NMR data for the product in separate tables with a labeled diagram 'H: chemical shift (experimental), chemical shift (literature), multiplet structure, integration, assignment 13C: chemical shift (experimental), chemical shift (literature), assignment In the current experiment, we will use a different electrophile (the tert.-butyl cation) to alkylate 1,4-dimethoxybenzene. This is a Friedel-Crafts Alkylation reaction. OCH3 (H;C),C. OCH3 (CH3),COH CH;COOH/H,SO4 H;CO H,CO C(CH3)3 Characterization IV • 13C-NMR Spectrum • Six signals from compounds and three lines from NMR solvent 8(ppm) Assignment 29.8 C(CH;); | C(CH;); OCH3 34.6 55.9 Arene-C ortho to OCH3 Arene-C attached to C(CH;); Arene-C attached to OCH; |CDCI, (three lines) 111.7 136,3 152.0 77 -1633

EBK A SMALL SCALE APPROACH TO ORGANIC L

4th Edition

ISBN:9781305446021

Author:Lampman

Publisher:Lampman

Chapter30: Resolution Of (6)-a-phenylethylamine And Determination Of Optical Purity

Section: Chapter Questions

Problem 5Q

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