L00 5) C1,H1,N IR 3000 1000 4D00 Spo 140 120 100 80 60 40 20 13C NMR Impurity Impurity N/A CDCI, 1Η NMR 3 2 TMS 5 Impurity 8 6 3 2

Introduction to General, Organic and Biochemistry
11th Edition
ISBN:9781285869759
Author:Frederick A. Bettelheim, William H. Brown, Mary K. Campbell, Shawn O. Farrell, Omar Torres
Publisher:Frederick A. Bettelheim, William H. Brown, Mary K. Campbell, Shawn O. Farrell, Omar Torres
Chapter23: Enzymes
Section: Chapter Questions
Problem 23.36P
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Step 1: Calculate the Index of Hydrogen Deficiency (IHD).

Step 2: Use IR to determine obvious functional groups.

Step 3: Use 1H-NMR to determine structural details. 

Step 4: Confirm the final structure using 13C-NMR.

 

Find and draw the structure and give supporting data.

TRANSHETTANCEI
L0
5) C1,H,N
IR
3000
2000
1000
400
500
140
120
100
80
60
40
20
13C NMR
Impurity
Impurity
N/A
CDCI,
1H NMR
3
2
TMS
5
1
Impurity
7
6
5
4
3
1
Transcribed Image Text:TRANSHETTANCEI L0 5) C1,H,N IR 3000 2000 1000 400 500 140 120 100 80 60 40 20 13C NMR Impurity Impurity N/A CDCI, 1H NMR 3 2 TMS 5 1 Impurity 7 6 5 4 3 1
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