FCompound 10 is a low-boiling liquid (boiling point 58 "C), that reacts with Br, in CCI, to form a 1,1,2,2-tetra bromide The Mass,RÄCÍTICAL SPECTROSCOPYFCompound 10 is a low-boiling liquid (boiling point 58 "C) that reacts with Br. in CCI, to form a 1,1,2,2-tetra bromiide TheR, and 'H NMR spectra, along with "C NMR data ve aiven below Flemental Analysis:C. 48 36. H. 4.06; contains halogen.Mass Spectrum397450 60140 150160 170180 190 2003040708090100 110 120 130mveInfrared SpectrumWave Number, cm 14000 1000 2500200015001300 1200 15D00 10c0900B007001512131415Wavelength, microns" Η NMRppm. 5Structurei"C Spectral Data:doublet, 80.4 ppmsinglet, 68.3 ppmtriplet, 347 ppin50.0mude02000 Brooks/Cole Publishing CompanyAbsorbance

M:M+2 (3:1 ) . Therefore chlorine present. 3300 cm-1 sp C-H present. Therefore the compound is…

Mass Spectrum 24 700 100 110 120 139 140 150 16O 170 18O 190 200 90 mie Infrared Spectrum Wave Number, cm 4000 000 2500 2000 IS0 1300 1200 1100 700 12 13 14 15 'H NMR Wavelongth, microns Strecture "C Spectral Data: doublet, 80.4 ppm singlet, 68.3 ppm triplet, 14pn 50.0m 02000 Brooks Cole Publishing Company Ausuasu aouequosay

Mass Spectrum 24 700 100 110 120 139 140 150 16O 170 18O 190 200 90 mie Infrared Spectrum Wave Number, cm 4000 000 2500 2000 IS0 1300 1200 1100 700 12 13 14 15 'H NMR Wavelongth, microns Strecture "C Spectral Data: doublet, 80.4 ppm singlet, 68.3 ppm triplet, 14pn 50.0m 02000 Brooks Cole Publishing Company Ausuasu aouequosay

Principles of Instrumental Analysis

7th Edition

ISBN:9781305577213

Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch

Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch

Chapter26: An Introduction To Chromatographic Separations

Section: Chapter Questions

Problem 26.19QAP

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